9-benzyl-1-(4-methoxybenzenesulfonyl)-3-methylene-5-(ptoluenesulfonyl)-1,5,9-triazacyclododecane

Base Information

Chemical Name:9-benzyl-1-(4-methoxybenzenesulfonyl)-3-methylene-5-(ptoluenesulfonyl)-1,5,9-triazacyclododecane
CAS No.:1322645-59-9
Molecular Formula:C₃₁H₃₉N₃O₅S₂
Molecular Weight:597.8
Hs Code.:

Synonyms:9-benzyl-1-(4-methoxybenzenesulfonyl)-3-methylene-5-(ptoluenesulfonyl)-1,5,9-triazacyclododecane

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Chemical Property of 9-benzyl-1-(4-methoxybenzenesulfonyl)-3-methylene-5-(ptoluenesulfonyl)-1,5,9-triazacyclododecane

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Technology Process of 9-benzyl-1-(4-methoxybenzenesulfonyl)-3-methylene-5-(ptoluenesulfonyl)-1,5,9-triazacyclododecane

There total 8 articles about 9-benzyl-1-(4-methoxybenzenesulfonyl)-3-methylene-5-(ptoluenesulfonyl)-1,5,9-triazacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-(N-benzyl-3-aminopropyl)-4-methylbenzenesulfonamide

: 1322645-59-9
9-benzyl-1-(4-methoxybenzenesulfonyl)-3-methylene-5-(ptoluenesulfonyl)-1,5,9-triazacyclododecane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; sodium iodide / acetonitrile / 24 h / Inert atmosphere; Reflux

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,4-di(diphenylphosphino)-butane / acetonitrile / 24 h / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium carbonate; 1,4-di(diphenylphosphino)-butane; sodium iodide; In acetonitrile;
DOI:10.1021/jm2002603

Reference yield:

: 193945-42-5
C₁₇H₂₀N₂O₂S

: 1322645-59-9
9-benzyl-1-(4-methoxybenzenesulfonyl)-3-methylene-5-(ptoluenesulfonyl)-1,5,9-triazacyclododecane

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / ethanol / 20 °C / Inert atmosphere

2: sodium carbonate; sodium iodide / acetonitrile / 24 h / Inert atmosphere; Reflux

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,4-di(diphenylphosphino)-butane / acetonitrile / 24 h / Inert atmosphere; Reflux

With sodium tetrahydroborate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium carbonate; 1,4-di(diphenylphosphino)-butane; sodium iodide; In ethanol; acetonitrile;
DOI:10.1021/jm2002603

Reference yield:

: 1094269-81-4
N-(3-bromo-propyl)-4-methoxy-benzenesulfonamide

: 1322645-59-9
9-benzyl-1-(4-methoxybenzenesulfonyl)-3-methylene-5-(ptoluenesulfonyl)-1,5,9-triazacyclododecane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; sodium iodide / acetonitrile / 24 h / Inert atmosphere; Reflux

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,4-di(diphenylphosphino)-butane / acetonitrile / 24 h / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium carbonate; 1,4-di(diphenylphosphino)-butane; sodium iodide; In acetonitrile;
DOI:10.1021/jm2002603