2-(2,5-dimethyl-1H-pyrrol-1-yl)-6-((3-(3-(2,5-dimethyl-1H-pyrrol-1-yl)propoxy)phenoxy)-methyl)-4-methylpyridine

Base Information

Chemical Name:2-(2,5-dimethyl-1H-pyrrol-1-yl)-6-((3-(3-(2,5-dimethyl-1H-pyrrol-1-yl)propoxy)phenoxy)-methyl)-4-methylpyridine
CAS No.:1450659-28-5
Molecular Formula:C₂₈H₃₃N₃O₂
Molecular Weight:443.589
Hs Code.:

Synonyms:2-(2,5-dimethyl-1H-pyrrol-1-yl)-6-((3-(3-(2,5-dimethyl-1H-pyrrol-1-yl)propoxy)phenoxy)-methyl)-4-methylpyridine

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Chemical Property of 2-(2,5-dimethyl-1H-pyrrol-1-yl)-6-((3-(3-(2,5-dimethyl-1H-pyrrol-1-yl)propoxy)phenoxy)-methyl)-4-methylpyridine

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Technology Process of 2-(2,5-dimethyl-1H-pyrrol-1-yl)-6-((3-(3-(2,5-dimethyl-1H-pyrrol-1-yl)propoxy)phenoxy)-methyl)-4-methylpyridine

There total 5 articles about 2-(2,5-dimethyl-1H-pyrrol-1-yl)-6-((3-(3-(2,5-dimethyl-1H-pyrrol-1-yl)propoxy)phenoxy)-methyl)-4-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-13-4
2,5-hexanedione

: 1450659-28-5
2-(2,5-dimethyl-1H-pyrrol-1-yl)-6-((3-(3-(2,5-dimethyl-1H-pyrrol-1-yl)propoxy)phenoxy)-methyl)-4-methylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 8 h / Reflux; Inert atmosphere

2: potassium carbonate / acetone / 8 h / Inert atmosphere; Reflux

3: potassium carbonate / acetone / 8 h / Inert atmosphere; Reflux

With potassium carbonate; toluene-4-sulfonic acid; In acetone; toluene;
DOI:10.1016/j.bmc.2013.06.014

Reference yield:

: 5407-87-4
2-Amino-4,6-dimethylpyridine

: 1450659-28-5
2-(2,5-dimethyl-1H-pyrrol-1-yl)-6-((3-(3-(2,5-dimethyl-1H-pyrrol-1-yl)propoxy)phenoxy)-methyl)-4-methylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / toluene / 8 h / Reflux; Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere

3.1: 1,2-dibromo-1,1,2,2-tetrafluoroethane; cesium fluoride / N,N-dimethyl-formamide / Inert atmosphere

4.1: potassium carbonate / acetone / 8 h / Inert atmosphere; Reflux

With n-butyllithium; 1,2-dibromo-1,1,2,2-tetrafluoroethane; potassium carbonate; toluene-4-sulfonic acid; cesium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.bmc.2013.06.014

Reference yield:

: 179554-66-6
2-(2,5-dimethyl-1H-pyrrol-1-yl)-4,6-dimethylpyridine

: 1450659-28-5
2-(2,5-dimethyl-1H-pyrrol-1-yl)-6-((3-(3-(2,5-dimethyl-1H-pyrrol-1-yl)propoxy)phenoxy)-methyl)-4-methylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: 1,2-dibromo-1,1,2,2-tetrafluoroethane; cesium fluoride / N,N-dimethyl-formamide / Inert atmosphere

3.1: potassium carbonate / acetone / 8 h / Inert atmosphere; Reflux

With n-butyllithium; 1,2-dibromo-1,1,2,2-tetrafluoroethane; potassium carbonate; cesium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2013.06.014