1-(carboxymethyl)-3(S)-<<1(S)-(ethoxycarbonyl)-3-phenylpropyl>amino>perhydroazocin-2-one hydrochloride

Base Information

Chemical Name:1-(carboxymethyl)-3(S)-<<1(S)-(ethoxycarbonyl)-3-phenylpropyl>amino>perhydroazocin-2-one hydrochloride
CAS No.:81874-36-4
Molecular Formula:C₂₁H₃₀N₂O₅*ClH
Molecular Weight:426.941
Hs Code.:

Synonyms:1-(carboxymethyl)-3(S)-<<1(S)-(ethoxycarbonyl)-3-phenylpropyl>amino>perhydroazocin-2-one hydrochloride

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Chemical Property of 1-(carboxymethyl)-3(S)-<<1(S)-(ethoxycarbonyl)-3-phenylpropyl>amino>perhydroazocin-2-one hydrochloride

Chemical Property:

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Technology Process of 1-(carboxymethyl)-3(S)-<<1(S)-(ethoxycarbonyl)-3-phenylpropyl>amino>perhydroazocin-2-one hydrochloride

There total 12 articles about 1-(carboxymethyl)-3(S)-<<1(S)-(ethoxycarbonyl)-3-phenylpropyl>amino>perhydroazocin-2-one hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32566-61-3
3-bromohexahydroazocin-2(1H)-one

: 81874-36-4
1-(carboxymethyl)-3(S)-<<1(S)-(ethoxycarbonyl)-3-phenylpropyl>amino>perhydroazocin-2-one hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / sodium azide / ethanol; H₂O

2: 76 percent / NaH / tetrahydrofuran / 1.5 h / Heating

3: 100 percent / H₂ / 10percent Pd/C

5: sodium acetate, sodium borohydride / ethanol

6: 4 N HCl / ethyl acetate

With hydrogenchloride; sodium tetrahydroborate; sodium azide; hydrogen; sodium acetate; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; ethyl acetate;
DOI:10.1021/jm00152a014

Reference yield:

: 32566-61-3
3-bromohexahydroazocin-2(1H)-one

: 81867-26-7,81874-36-4
(-)-1-(carboxymethyl)-3(R)-<<1(R)-(ethoxycarbonyl)-3-phenylpropyl>amino>perhydroazocin-2-one hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / sodium azide / ethanol; H₂O

2: 76 percent / NaH / tetrahydrofuran / 1.5 h / Heating

3: 100 percent / H₂ / 10percent Pd/C

5: sodium acetate, sodium borohydride / ethanol

6: 4 N HCl / ethyl acetate

With hydrogenchloride; sodium tetrahydroborate; sodium azide; hydrogen; sodium acetate; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; ethyl acetate;
DOI:10.1021/jm00152a014

Reference yield:

: 81867-12-1
3-azidohexahydro-2(1H)-azocinone

: 81874-36-4
1-(carboxymethyl)-3(S)-<<1(S)-(ethoxycarbonyl)-3-phenylpropyl>amino>perhydroazocin-2-one hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / NaH / tetrahydrofuran / 1.5 h / Heating

2: 100 percent / H₂ / 10percent Pd/C

4: sodium acetate, sodium borohydride / ethanol

5: 4 N HCl / ethyl acetate

With hydrogenchloride; sodium tetrahydroborate; hydrogen; sodium acetate; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate;
DOI:10.1021/jm00152a014