[5-(N-p-fluorophenylamino)methyl-4-phenyl-1,2,4-triazol-3-yl]thioglycolylhydrazide

Base Information

Chemical Name:[5-(N-p-fluorophenylamino)methyl-4-phenyl-1,2,4-triazol-3-yl]thioglycolylhydrazide
CAS No.:680594-43-8
Molecular Formula:C₁₇H₁₇FN₆OS
Molecular Weight:372.426
Hs Code.:

Synonyms:[5-(N-p-fluorophenylamino)methyl-4-phenyl-1,2,4-triazol-3-yl]thioglycolylhydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [5-(N-p-fluorophenylamino)methyl-4-phenyl-1,2,4-triazol-3-yl]thioglycolylhydrazide

Chemical Property:

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Technology Process of [5-(N-p-fluorophenylamino)methyl-4-phenyl-1,2,4-triazol-3-yl]thioglycolylhydrazide

There total 5 articles about [5-(N-p-fluorophenylamino)methyl-4-phenyl-1,2,4-triazol-3-yl]thioglycolylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 333311-80-1
ethyl [5-(N-p-fluorophenylamino)methyl-4-phenyl-1,2,4-triazol-3-yl]thioglycolate

: 680594-43-8
[5-(N-p-fluorophenylamino)methyl-4-phenyl-1,2,4-triazol-3-yl]thioglycolylhydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 3h; Heating;

Reference yield:

: 710-31-6
2-[(4-fluorophenyl)amino]acetohydrazide

: 680594-43-8
[5-(N-p-fluorophenylamino)methyl-4-phenyl-1,2,4-triazol-3-yl]thioglycolylhydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 86 percent / ethanol / 1 h / Heating

2.1: 77 percent / aq. NaOH / 3 h / Heating

3.1: NaOH / ethanol / 0.75 h / Heating

3.2: 70 percent / ethanol / 4 h / Heating

4.1: 80 percent / hydrazine hydrate / ethanol / 3 h / Heating

With sodium hydroxide; hydrazine hydrate; In ethanol;

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 680594-43-8
[5-(N-p-fluorophenylamino)methyl-4-phenyl-1,2,4-triazol-3-yl]thioglycolylhydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 86 percent / ethanol / 1 h / Heating

2.1: 77 percent / aq. NaOH / 3 h / Heating

3.1: NaOH / ethanol / 0.75 h / Heating

3.2: 70 percent / ethanol / 4 h / Heating

4.1: 80 percent / hydrazine hydrate / ethanol / 3 h / Heating

With sodium hydroxide; hydrazine hydrate; In ethanol;