8-(4-(4-Nitrophenyl)-3-azabutyl)-2,6-dioxo-1,4,7,10-tetraazacyclododecane

Base Information

Chemical Name:8-(4-(4-Nitrophenyl)-3-azabutyl)-2,6-dioxo-1,4,7,10-tetraazacyclododecane
CAS No.:151990-89-5
Molecular Formula:C₁₇H₂₆N₆O₄
Molecular Weight:378.431
Hs Code.:

Synonyms:8-(4-(4-Nitrophenyl)-3-azabutyl)-2,6-dioxo-1,4,7,10-tetraazacyclododecane

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Chemical Property of 8-(4-(4-Nitrophenyl)-3-azabutyl)-2,6-dioxo-1,4,7,10-tetraazacyclododecane

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Technology Process of 8-(4-(4-Nitrophenyl)-3-azabutyl)-2,6-dioxo-1,4,7,10-tetraazacyclododecane

There total 4 articles about 8-(4-(4-Nitrophenyl)-3-azabutyl)-2,6-dioxo-1,4,7,10-tetraazacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 6290-05-7
Diethyl iminodiacetate

: 152014-59-0
5,9-Diamino-1-(4-nitrophenyl)-2,7-diazanonane

: 151990-89-5
8-(4-(4-Nitrophenyl)-3-azabutyl)-2,6-dioxo-1,4,7,10-tetraazacyclododecane

Guidance literature:: In methanol; for 240h; Heating;
DOI:10.1021/jo00076a062

Reference yield:

: 2-Amino-N-(4-nitro-benzyl)-succinamic acid

: 151990-89-5
8-(4-(4-Nitrophenyl)-3-azabutyl)-2,6-dioxo-1,4,7,10-tetraazacyclododecane

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 2 h / Ambient temperature

2: 41 percent / BH₃ / tetrahydrofuran / 24 h / Heating

3: 9 percent / methanol / 240 h / Heating

With borane; In tetrahydrofuran; methanol;
DOI:10.1021/jo00076a062

Reference yield:

: 151990-88-4
5,9-Diamino-1-(4-nitrophenyl)-3,6-dioxo-2,7-diazanonane

: 151990-89-5
8-(4-(4-Nitrophenyl)-3-azabutyl)-2,6-dioxo-1,4,7,10-tetraazacyclododecane

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / BH₃ / tetrahydrofuran / 24 h / Heating

2: 9 percent / methanol / 240 h / Heating

With borane; In tetrahydrofuran; methanol;
DOI:10.1021/jo00076a062