1-(2-benzylselenenyl-5-methoxyphenyl)-3,7,11,15-tetramethyl-3-hexadecanol

Base Information

Chemical Name:1-(2-benzylselenenyl-5-methoxyphenyl)-3,7,11,15-tetramethyl-3-hexadecanol
CAS No.:371114-90-8
Molecular Formula:C₃₄H₅₄O₂Se
Molecular Weight:573.762
Hs Code.:

Synonyms:1-(2-benzylselenenyl-5-methoxyphenyl)-3,7,11,15-tetramethyl-3-hexadecanol

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Chemical Property of 1-(2-benzylselenenyl-5-methoxyphenyl)-3,7,11,15-tetramethyl-3-hexadecanol

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Technology Process of 1-(2-benzylselenenyl-5-methoxyphenyl)-3,7,11,15-tetramethyl-3-hexadecanol

There total 5 articles about 1-(2-benzylselenenyl-5-methoxyphenyl)-3,7,11,15-tetramethyl-3-hexadecanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 88591-64-4
4,8,12-trimethyltridecyl bromide

: 371114-88-4
2-(2-benzylselenyl-5-methoxyphenyl)ethyl methyl ketone

: 371114-90-8
1-(2-benzylselenenyl-5-methoxyphenyl)-3,7,11,15-tetramethyl-3-hexadecanol

Guidance literature:: 4,8,12-trimethyltridecyl bromide; With magnesium; In diethyl ether; for 5h; Heating;

2-(2-benzylselenyl-5-methoxyphenyl)ethyl methyl ketone; In diethyl ether; at 20 ℃; for 18h; Further stages.;
DOI:10.1021/jo010274k

Reference yield:

: 371114-86-2
4-(2-bromo-5-methoxyphenyl)-2-butanone

: 371114-90-8
1-(2-benzylselenenyl-5-methoxyphenyl)-3,7,11,15-tetramethyl-3-hexadecanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 97 percent / p-TsOH / benzene / Heating

2.1: t-BuLi / tetrahydrofuran / 0.5 h / 0 °C

2.2: Se / tetrahydrofuran / 0.5 h / 20 °C

2.3: tetrahydrofuran / 20 °C

3.1: 674 mg / aq. HCl / tetrahydrofuran / 18 h / 20 °C

4.1: Mg / diethyl ether / 5 h / Heating

4.2: 54 percent / diethyl ether / 18 h / 20 °C

With hydrogenchloride; tert.-butyl lithium; toluene-4-sulfonic acid; magnesium; In tetrahydrofuran; diethyl ether; benzene;
DOI:10.1021/jo010274k

Reference yield:

: 371114-87-3
2-[2-(2-bromo-5-methoxyphenyl)ethyl]-2-methyl-1,3-dioxolane

: 371114-90-8
1-(2-benzylselenenyl-5-methoxyphenyl)-3,7,11,15-tetramethyl-3-hexadecanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: t-BuLi / tetrahydrofuran / 0.5 h / 0 °C

1.2: Se / tetrahydrofuran / 0.5 h / 20 °C

1.3: tetrahydrofuran / 20 °C

2.1: 674 mg / aq. HCl / tetrahydrofuran / 18 h / 20 °C

3.1: Mg / diethyl ether / 5 h / Heating

3.2: 54 percent / diethyl ether / 18 h / 20 °C

With hydrogenchloride; tert.-butyl lithium; magnesium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo010274k