(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester

Base Information

Chemical Name:(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester
CAS No.:81149-15-7
Molecular Formula:C₂₄H₂₆N₂O₅
Molecular Weight:422.481
Hs Code.:

(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzo<F>chinolin-2-carbonsaeuremethylester

Synonyms:(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester

Suppliers and Price of (2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester

There total 2 articles about (2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 65291-20-5
(2R,4aR,10bR)-7-Amino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester

: 81149-15-7
(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester

Guidance literature:: In tetrahydrofuran; pyridine; at 20 ℃;

Reference yield:

: 3006-19-7,5143-94-2,35470-53-2,77842-02-5,87247-99-2,96648-31-6,96648-32-7
9,10-dihydrolysergic acid methyl ester

: 81149-15-7
(2R,4aR,10bR)-7-Benzyloxycarbonylamino-1,2,3,4,4a,5,6,10b-octahydro-6-oxobenzochinolin-2-carbonsaeuremethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.8 g / NaIO₄ / methanol; H₂O / 64 h / -2 °C

2: 72 percent / tetrahydrofuran; pyridine / 20 °C

With sodium periodate; In tetrahydrofuran; pyridine; methanol; water;