C₄₄H₆₄N₆O₉

Base Information

Chemical Name:C₄₄H₆₄N₆O₉
CAS No.:1391035-20-3
Molecular Formula:C₄₄H₆₄N₆O₉
Molecular Weight:821.027
Hs Code.:

C<sub>44</sub>H<sub>64</sub>N<sub>6</sub>O<sub>9</sub>

Synonyms:C₄₄H₆₄N₆O₉

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Chemical Property of C₄₄H₆₄N₆O₉

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Technology Process of C₄₄H₆₄N₆O₉

There total 13 articles about C₄₄H₆₄N₆O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.3%

: 1391035-19-0
C₁₀H₂₁N₃O₃*ClH

: 1391035-04-3
C₃₄H₄₅N₃O₇

: 1391035-20-3
C₄₄H₆₄N₆O₉

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ml300083p

Reference yield:

: 108-69-0
3,5-dimethylaminoaniline

: 1391035-20-3
C₄₄H₆₄N₆O₉

Guidance literature:: Multi-step reaction with 6 steps

1: bromine / dichloromethane / 1.5 h

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / N,N-dimethyl-formamide / 16 h / 80 °C / Inert atmosphere

3: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / tetrahydrofuran; water / 0.5 h / 80 °C / Inert atmosphere; Microwave irradiation

4: sodium hydroxide / methanol; water / 12 h / 20 °C

5: tetrahydrofuran / 12 h / 20 °C / Cooling

6: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; bromine; potassium acetate; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 3: |Suzuki Coupling;
DOI:10.1021/ml300083p

Reference yield:

: 78022-19-2
dimethyl (4-carbomethoxybenzyl)phosphonate

: 1391035-20-3
C₄₄H₆₄N₆O₉

Guidance literature:: Multi-step reaction with 8 steps

1: lithium diisopropyl amide / tetrahydrofuran / 12 h / -78 - 20 °C

2: bromine; potassium carbonate / dichloromethane / 1.5 h / 0 - 20 °C

3: sodium hydroxide / methanol / 3 h / 40 °C

4: dmap; thionyl chloride / dichloromethane / 12 h / -20 - 20 °C

5: bis-triphenylphosphine-palladium(II) chloride; potassium carbonate / tetrahydrofuran; water / 0.5 h / 80 °C / Inert atmosphere; Microwave irradiation

6: sodium hydroxide / methanol; water / 12 h / 20 °C

7: tetrahydrofuran / 12 h / 20 °C / Cooling

8: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; thionyl chloride; bromine; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 1: |Wittig-Horner Reaction / 5: |Suzuki Coupling;
DOI:10.1021/ml300083p