3,3-diphenyl-3H-4,9,11-trioxa-7,13-diaza-benzo[a]cyclopenta[i]anthracene

Base Information

Chemical Name:3,3-diphenyl-3H-4,9,11-trioxa-7,13-diaza-benzo[a]cyclopenta[i]anthracene
CAS No.:314727-86-1
Molecular Formula:C₂₈H₁₈N₂O₃
Molecular Weight:430.463
Hs Code.:

3,3-diphenyl-3<i>H</i>-4,9,11-trioxa-7,13-diaza-benzo[<i>a</i>]cyclopenta[<i>i</i>]anthracene

Synonyms:3,3-diphenyl-3H-4,9,11-trioxa-7,13-diaza-benzo[a]cyclopenta[i]anthracene

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Chemical Property of 3,3-diphenyl-3H-4,9,11-trioxa-7,13-diaza-benzo[a]cyclopenta[i]anthracene

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Technology Process of 3,3-diphenyl-3H-4,9,11-trioxa-7,13-diaza-benzo[a]cyclopenta[i]anthracene

There total 5 articles about 3,3-diphenyl-3H-4,9,11-trioxa-7,13-diaza-benzo[a]cyclopenta[i]anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1,3-dioxa-5,10-diaza-cyclopenta[b]anthracen-7-ol

: 1210-39-5
3,3-diphenyl-2-propenal

: 314727-86-1
3,3-diphenyl-3H-4,9,11-trioxa-7,13-diaza-benzo[a]cyclopenta[i]anthracene

Guidance literature:: With titanium(IV) tetraethanolate; In toluene;
DOI:10.1080/10587250008023821

Reference yield:

: 7-methoxy-[1,3]dioxolo[4,5-b]phenazine

: 314727-86-1
3,3-diphenyl-3H-4,9,11-trioxa-7,13-diaza-benzo[a]cyclopenta[i]anthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / 9-bromo-9-borabicyclo[3.3.1]nonane / CH₂Cl₂ / 24 h / 0 °C

2: 54 percent / Ti(OEt)4 / toluene

With B-Br-9-BBN; titanium(IV) tetraethanolate; In dichloromethane; toluene;
DOI:10.1080/10587250008023821

Reference yield:

: 13161-92-7
2,3-dihydroxy-6-methoxyphenazine

: 314727-86-1
3,3-diphenyl-3H-4,9,11-trioxa-7,13-diaza-benzo[a]cyclopenta[i]anthracene

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / CsF / dimethylformamide

2: 79 percent / 9-bromo-9-borabicyclo[3.3.1]nonane / CH₂Cl₂ / 24 h / 0 °C

3: 54 percent / Ti(OEt)4 / toluene

With B-Br-9-BBN; titanium(IV) tetraethanolate; cesium fluoride; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1080/10587250008023821