Technology Process of C11H10F3N3O
There total 6 articles about C11H10F3N3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
In
ethanol;
for 4h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium nitrite; tetrafluoroboric acid / water / 0.5 h / 0 - 5 °C
2.1: pyridine / water / 0.5 h / -5 °C
3.1: triethylamine; bicyclo[2.2.1]hepta-2,5-diene / toluene / 1 h / 70 °C
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C
4.2: 0 °C
5.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 4 h / 0 - 20 °C
5.2: 20 °C
6.1: hydrazine hydrate / ethanol / 4 h / Reflux
With
pyridine; lithium aluminium tetrahydride; tetrafluoroboric acid; hydrazine hydrate; bicyclo[2.2.1]hepta-2,5-diene; triethylamine; triphenylphosphine; sodium nitrite; diethylazodicarboxylate;
In
tetrahydrofuran; ethanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine; bicyclo[2.2.1]hepta-2,5-diene / toluene / 1 h / 70 °C
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C
2.2: 0 °C
3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 4 h / 0 - 20 °C
3.2: 20 °C
4.1: hydrazine hydrate / ethanol / 4 h / Reflux
With
lithium aluminium tetrahydride; hydrazine hydrate; bicyclo[2.2.1]hepta-2,5-diene; triethylamine; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; ethanol; toluene;
