(S)-(-)-(2E,6E)-9-(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl bromide

Base Information

Chemical Name:(S)-(-)-(2E,6E)-9-(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl bromide
CAS No.:850884-89-8
Molecular Formula:C₂₀H₃₃Br
Molecular Weight:353.386
Hs Code.:

Synonyms:(S)-(-)-(2E,6E)-9-(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl bromide

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Chemical Property of (S)-(-)-(2E,6E)-9-(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl bromide

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Technology Process of (S)-(-)-(2E,6E)-9-(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl bromide

There total 1 articles about (S)-(-)-(2E,6E)-9-(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 69903-57-7
(S)-(+)-(2E,6E)-9-(2,2-dimethyl-6-methylenencyclohexyl)-3,7-dimethyl-2,6-nonadien-1-ol

: 850884-89-8
(S)-(-)-(2E,6E)-9-(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl bromide

Guidance literature:: With phosphorus tribromide; In diethyl ether; at 0 ℃; for 3h;
DOI:10.1039/b417471b

Reference yield:

: 850884-89-8
(S)-(-)-(2E,6E)-9-(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl bromide

: 13300-29-3
N⁶-methoxy-9-methyl-9H-purin-6-amine

: (S)-(2'E,6'E)-N-[(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl]-N-methoxy-9-methyl-9H-purin-6-amine

: (S)-(2'E,6'E)-6-(methoxyamino)-9-methyl-7-[(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl]-7H-purinium chloride

Guidance literature:: (S)-(-)-(2E,6E)-9-(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl bromide; N⁶-methoxy-9-methyl-9H-purin-6-amine; In N,N-dimethyl acetamide; at 50 ℃; for 21h;

With Amberlite-Cl; In methanol;
DOI:10.1039/b417471b

Reference yield:

: 850884-89-8
(S)-(-)-(2E,6E)-9-(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl bromide

: (S)-(2'E,6'E)-6-amino-9-methyl-7-[(2,2-dimethyl-6-methylenecyclohexyl)-3,7-dimethyl-2,6-nonadien-1-yl]-7H-purinium chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-acetamide / 21 h / 50 °C

1.2: 62 mg / Amberlite-Cl / aq. methanol

2.1: 89 percent / Zn; aq. AcOH / methanol / 15 h / 60 °C

With acetic acid; zinc; In methanol; N,N-dimethyl acetamide;
DOI:10.1039/b417471b