cis-1-(2-fluorophenyl)-3-methoxycarbonyl-1,2,3,4-tetrahydro-β-carboline

Base Information

Chemical Name:cis-1-(2-fluorophenyl)-3-methoxycarbonyl-1,2,3,4-tetrahydro-β-carboline
CAS No.:238428-21-2
Molecular Formula:C₁₉H₁₇FN₂O₂
Molecular Weight:324.355
Hs Code.:

Synonyms:cis-1-(2-fluorophenyl)-3-methoxycarbonyl-1,2,3,4-tetrahydro-β-carboline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-1-(2-fluorophenyl)-3-methoxycarbonyl-1,2,3,4-tetrahydro-β-carboline

Chemical Property:

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Technology Process of cis-1-(2-fluorophenyl)-3-methoxycarbonyl-1,2,3,4-tetrahydro-β-carboline

There total 3 articles about cis-1-(2-fluorophenyl)-3-methoxycarbonyl-1,2,3,4-tetrahydro-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 7524-52-9,26988-71-6,5619-09-0,14907-27-8,41222-70-2,67557-19-1,109492-62-8
(S)-tryptophan methyl ester hydrochloride

: 446-52-6
2-Fluorobenzaldehyde

: 238428-21-2
cis-1-(2-fluorophenyl)-3-methoxycarbonyl-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: With sodium carbonate; In methanol;
DOI:10.1016/S0968-0896(99)00050-4

Reference yield:

: 446-52-6
2-Fluorobenzaldehyde

: 4299-70-1
L-tryptophan methyl ester

: 238428-21-2
cis-1-(2-fluorophenyl)-3-methoxycarbonyl-1,2,3,4-tetrahydro-β-carboline

: trans-1-(2-fluorophenyl)-3-methoxycarbonyl-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: With 1,1,1,3',3',3'-hexafluoro-propanol; for 20h; Overall yield = 92 %; Reflux; Inert atmosphere;
DOI:10.1039/c4ra03628j