C₄₅H₇₄O₆Si₂

Base Information

Chemical Name:C₄₅H₇₄O₆Si₂
CAS No.:1375412-54-6
Molecular Formula:C₄₅H₇₄O₆Si₂
Molecular Weight:767.25
Hs Code.:

C<sub>45</sub>H<sub>74</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₄₅H₇₄O₆Si₂

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Chemical Property of C₄₅H₇₄O₆Si₂

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Technology Process of C₄₅H₇₄O₆Si₂

There total 31 articles about C₄₅H₇₄O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1375412-36-4
C₄₇H₇₈O₆Si₂

: 1375412-54-6
C₄₅H₇₄O₆Si₂

Guidance literature:: C₄₇H₇₈O₆Si₂; With 2,3,5,6-tetrafluoro-1,4-benzoquinone; Grela's catalyst; In dichloromethane; at 60 ℃; for 3h; Inert atmosphere;

With potassium 2-isocyanoacetate; In methanol; dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/anie.201108692

Reference yield:

: 1375412-36-4
C₄₇H₇₈O₆Si₂

: 1375412-55-7
C₃₈H₆₈O₆Si₂

: 1375412-54-6
C₄₅H₇₄O₆Si₂

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,3,5,6-tetrafluoro-1,4-benzoquinone; In toluene; at 90 ℃; for 1.5h;
DOI:10.1002/anie.201108692

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 1375412-54-6
C₄₅H₇₄O₆Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

2.1: copper(l) iodide / tetrahydrofuran; dimethyl sulfate / 3 h / -30 °C

3.1: sodium periodate / tetrahydrofuran; water / 6 h / 20 °C

4.1: N-chloro-succinimide; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt / acetonitrile / 2.5 h / 0 °C

4.2: 0.5 h

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

5.2: 1 h / -50 - -45 °C

5.3: 2 h / -70 - 0 °C

6.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

7.1: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

8.1: dmap; 2,4,6-trichlorobenzoyl chloride; dihydropyrimidinone / toluene / 7 h / 0 - 20 °C / Inert atmosphere

9.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenyl-arsane / N,N-dimethyl-formamide / 1.5 h

10.1: Grela's catalyst; 2,3,5,6-tetrafluoro-1,4-benzoquinone / dichloromethane / 3 h / 60 °C / Inert atmosphere

10.2: 2 h / 20 °C

With 2,6-dimethylpyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium periodate; N-chloro-succinimide; N-Bromosuccinimide; copper(l) iodide; n-butyllithium; samarium diiodide; triphenyl-arsane; 2,3,5,6-tetrafluoro-1,4-benzoquinone; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt; 2,4,6-trichlorobenzoyl chloride; Grela's catalyst; silver perchlorate; 3-chloro-benzenecarboperoxoic acid; dihydropyrimidinone; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; dimethyl sulfate; acetonitrile; 5.3: Brook rearrangement / 7.1: Evans-Tishchenko reduction / 9.1: Stille coupling;
DOI:10.1002/anie.201108692