2,3,4,5,6,7-hexa-O-benzyl-6-D-glycero-2,3,4,5-D-galacto-heptose

Base Information

• Chemical Name: 2,3,4,5,6,7-hexa-O-benzyl-6-D-glycero-2,3,4,5-D-galacto-heptose
• CAS No.: 155193-88-7
• Molecular Formula: C₄₉H₅₀O₇
• Molecular Weight: 750.932
• Mol file: 155193-88-7.mol

Synonyms:2,3,4,5,6,7-hexa-O-benzyl-6-D-glycero-2,3,4,5-D-galacto-heptose

Chemical Property of 2,3,4,5,6,7-hexa-O-benzyl-6-D-glycero-2,3,4,5-D-galacto-heptose

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,4,5,6,7-hexa-O-benzyl-6-D-glycero-2,3,4,5-D-galacto-heptose

There total 1 articles about 2,3,4,5,6,7-hexa-O-benzyl-6-D-glycero-2,3,4,5-D-galacto-heptose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C53H60O6S2 (155193-87-6) → 2,3,4,5,6,7-hexa-O-benzyl-6-D-glycero-2,3,4,5-D-galacto-heptose (155193-88-7)

Guidance literature:

With sodium carbonate; methyl iodide; In water; acetonitrile;

DOI:10.1246/cl.1994.129

Reference yield: 80.0%

methyl 2-(benzyloxycarbonylamino)-2-(diethyloxyphosphoryl)acetate (114684-69-4) + 2,3,4,5,6,7-hexa-O-benzyl-6-D-glycero-2,3,4,5-D-galacto-heptose (155193-88-7) → (Z)-(4S,5R,6R,7R,8R)-4,5,6,7,8,9-Hexakis-benzyloxy-2-benzyloxycarbonylamino-non-2-enoic acid methyl ester

Guidance literature:

With sodium hydride; In dichloromethane;

DOI:10.1246/cl.1994.129

Reference yield:

2,3,4,5,6,7-hexa-O-benzyl-6-D-glycero-2,3,4,5-D-galacto-heptose (155193-88-7) → (4S,5R,6R,7R,8R)-4,5,6,7,8,9-Hexakis-benzyloxy-2-oxo-nonanoic acid methyl ester (155193-91-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / NaH / CH₂Cl₂

2: 40 percent / H₂ / 5percent Pd/C / benzene

With hydrogen; sodium hydride; palladium on activated charcoal; In dichloromethane; benzene;

DOI:10.1246/cl.1994.129

upstream raw materials:

C₅₃H₆₀O₆S₂

Downstream raw materials:

(4S,5R,6R,7R,8R)-4,5,6,7,8,9-Hexakis-benzyloxy-2-oxo-nonanoic acid methyl ester