Technology Process of C41H63N3Si
There total 16 articles about C41H63N3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; diisopropylamine; triphenylphosphine;
bis(dibenzylideneacetone)-palladium(0);
In
tetrahydrofuran;
at 23 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 87 percent / 1 N NaOH / tetrahydrofuran / 2 h / Heating
2: AlCl3 / CS2 / 3 h / 70 °C
3: 3 N NaOH
4: 1.) t-BuONO, BF3-OEt2, 2.) K2CO3 / 1.) CH2Cl2, 0 deg C, 30 min, 2.) 1 h
6: 92 percent / MeI / 120 °C
7: 78 percent / Pd(dba)2, Ph3P, CuI, i-Pr2NH / tetrahydrofuran
With
sodium hydroxide; copper(l) iodide; aluminium trichloride; tert.-butylnitrite; boron trifluoride diethyl etherate; potassium carbonate; diisopropylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0); methyl iodide;
In
tetrahydrofuran; carbon disulfide;
DOI:10.1021/jo962336q
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) t-BuONO, BF3-OEt2, 2.) K2CO3 / 1.) CH2Cl2, 0 deg C, 30 min, 2.) 1 h
3: 92 percent / MeI / 120 °C
4: 78 percent / Pd(dba)2, Ph3P, CuI, i-Pr2NH / tetrahydrofuran
With
copper(l) iodide; tert.-butylnitrite; boron trifluoride diethyl etherate; potassium carbonate; diisopropylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0); methyl iodide;
In
tetrahydrofuran;
DOI:10.1021/jo962336q