2-β-(N-Phenylthioureido)-N'-ethyl-1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4>indole

Base Information

Chemical Name:2-β-(N-Phenylthioureido)-N'-ethyl-1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4>indole
CAS No.:72593-32-9
Molecular Formula:C₂₃H₂₇N₅S
Molecular Weight:405.567
Hs Code.:

Synonyms:2-β-(N-Phenylthioureido)-N'-ethyl-1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4>indole

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Chemical Property of 2-β-(N-Phenylthioureido)-N'-ethyl-1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4>indole

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Technology Process of 2-β-(N-Phenylthioureido)-N'-ethyl-1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4>indole

There total 3 articles about 2-β-(N-Phenylthioureido)-N'-ethyl-1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4>indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.7%

: 91119-31-2
2-β-Aminoethyl-1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4-b>indole

: 103-72-0
phenyl isothiocyanate

: 72593-32-9
2-β-(N-Phenylthioureido)-N'-ethyl-1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4>indole

Guidance literature:: In tetrahydrofuran; at 30 ℃; for 3h;

Reference yield:

: 91119-30-1
2-Cyanomethyl 1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4-b>indol

: 72593-32-9
2-β-(N-Phenylthioureido)-N'-ethyl-1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4>indole

Guidance literature:: Multi-step reaction with 2 steps

1: 78.6 percent / LAH / tetrahydrofuran / 10 h / Heating

2: 94.7 percent / tetrahydrofuran / 3 h / 30 °C

With lithium aluminium tetrahydride; In tetrahydrofuran;

Reference yield:

: 55344-28-0
1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4-b>indole

: 72593-32-9
2-β-(N-Phenylthioureido)-N'-ethyl-1,2,3,4,6,7,12,12a-octahydropyrazino<2',1':6,1>pyrido<3,4>indole

Guidance literature:: Multi-step reaction with 3 steps

1: 76.5 percent / Na₂CO₃ / dimethylformamide / 24 h / 30 °C

2: 78.6 percent / LAH / tetrahydrofuran / 10 h / Heating

3: 94.7 percent / tetrahydrofuran / 3 h / 30 °C

With lithium aluminium tetrahydride; sodium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;