2,3-Dichlorothioanisole

Base Information

Chemical Name:2,3-Dichlorothioanisole
CAS No.:17733-25-4
Molecular Formula:C7H6Cl2S
Molecular Weight:193.097
Hs Code.:2930909090
DSSTox Substance ID:DTXSID70938922
Nikkaji Number:J3.209.357D
Wikidata:Q82915342
Mol file:17733-25-4.mol

Synonyms:2,3-Dichlorothioanisole;17733-25-4;1,2-Dichloro-3-(methylsulfanyl)benzene;(2,3-Dichlorophenyl)(methyl)sulfane;1,2-dichloro-3-methylsulfanylbenzene;Sulfide, 2,3-dichlorophenyl methyl;Benzene, 1,2-dichloro-3-(methylthio)-;dichlorothioanisol;SCHEMBL1146294;DTXSID70938922;YSQBVIAGPLXQJH-UHFFFAOYSA-N;2,3-Dichlorophenyl(methyl)sulfane;MFCD03789169;AKOS006278382;FS-5280;CS-0193487;FT-0710433;E89705

Suppliers and Price of 2,3-Dichlorothioanisole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
(2,3-Dichlorophenyl)(methyl)sulfane 97%
5g
$ 367.00

AOBChem
1,2-Dichloro-3-(methylsulfanyl)benzene 96%
5g
$ 327.00

AOBChem
1,2-Dichloro-3-(methylsulfanyl)benzene 95%
1g
$ 91.00

AOBChem
1,2-Dichloro-3-(methylsulfanyl)benzene 96%
500mg
$ 65.00

AOBChem
1,2-Dichloro-3-(methylsulfanyl)benzene 95%
100g
$ 3022.00

AOBChem
1,2-Dichloro-3-(methylsulfanyl)benzene 96%
50g
$ 1890.00

AOBChem
1,2-Dichloro-3-(methylsulfanyl)benzene 95%
25g
$ 1092.00

AOBChem
1,2-Dichloro-3-(methylsulfanyl)benzene 96%
10g
$ 556.00

American Custom Chemicals Corporation
2,3-DICHLOROTHIOANISOLE 95.00%
5MG
$ 500.09

Total 2 raw suppliers

Chemical Property of 2,3-Dichlorothioanisole

Chemical Property:

Boiling Point:242.0±30.0 °C(Predicted)
PSA：25.30000
Density:1.35±0.1 g/cm3(Predicted)
LogP:3.71530
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:191.9567268
Heavy Atom Count:10
Complexity:108

Purity/Quality:

99% ^*data from raw suppliers

(2,3-Dichlorophenyl)(methyl)sulfane 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CSC1=C(C(=CC=C1)Cl)Cl

Technology Process of 2,3-Dichlorothioanisole

There total 4 articles about 2,3-Dichlorothioanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 17231-95-7
2,3-dichlorobenzenethiol

: 77-78-1
dimethyl sulfate

: 17733-25-4
1,2-Dichlor-3-(methylthio)benzol

Guidance literature:: With sodium hydroxide; In hexane; at 0 - 110 ℃; for 2h;

Reference yield: 40.0%

: 137092-25-2
Dithiopivalinsaeure-2,3-dichlorphenylester

: 40920-16-9
methyl dithiopivalate

: 17733-25-4
1,2-Dichlor-3-(methylthio)benzol

Guidance literature:: In N,N-dimethyl-formamide; cathodic reduction (and methylation of the product mixture), Hg cathode;

Reference yield:

: 106418-95-5
2,3-Dichloro-benzenediazonium; hydrogen sulfate

: 17733-25-4
1,2-Dichlor-3-(methylthio)benzol

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / Na₂CO₃ / H₂O; diethyl ether / 1.) cooling with ice, 10 min, 2.) to r.t.

2: 40 percent / dimethylformamide / cathodic reduction (and methylation of the product mixture), Hg cathode

With sodium carbonate; In diethyl ether; water; N,N-dimethyl-formamide;