C₆₆H₄₅N

Base Information

Chemical Name:C₆₆H₄₅N
CAS No.:1439381-57-3
Molecular Formula:C₆₆H₄₅N
Molecular Weight:852.09
Hs Code.:

Synonyms:C₆₆H₄₅N

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Chemical Property of C₆₆H₄₅N

Chemical Property:

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Technology Process of C₆₆H₄₅N

There total 3 articles about C₆₆H₄₅N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1439381-53-9
tris{4-[(E)-2-(4-iodophenyl)vinyl]phenyl}amine

: 536-74-3
phenylacetylene

: 1439381-57-3
C₆₆H₄₅N

Guidance literature:: tris{4-[(E)-2-(4-iodophenyl)vinyl]phenyl}amine; With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In toluene; for 0.25h; Inert atmosphere;

phenylacetylene; In toluene; at 80 ℃; Inert atmosphere;
DOI:10.1021/ma401085q

Reference yield:

: 603-34-9
N,N-diphenylaminobenzene

: 1439381-57-3
C₆₆H₄₅N

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 95 °C

2.1: potassium tert-butylate / tetrahydrofuran / Reflux

3.1: copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 0.25 h / Inert atmosphere

3.2: 80 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium tert-butylate; triethylamine; trichlorophosphate; In tetrahydrofuran; toluene; 1.1: |Vilsmeier-Haack Formylation / 2.1: |Horner-Wadsworth-Emmons Olefination / 3.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ma401085q

Reference yield:

: 119001-43-3
tris(4-formylphenyl)amine

: 1439381-57-3
C₆₆H₄₅N

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / Reflux

2.1: copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 0.25 h / Inert atmosphere

2.2: 80 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium tert-butylate; triethylamine; In tetrahydrofuran; toluene; 1.1: |Horner-Wadsworth-Emmons Olefination / 2.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ma401085q