N₄-(2,2-dimethyl-4-[(di-tert-butyl phosphonoxy)dideuteromethyl]-3-oxo-5-pyrido[1,4]oxazin-6-yl)-5-fluoro-N₂-(3,4,5-trimethoxyphenyl)-2,4-pyrimidinediamine

Base Information

• Chemical Name: N₄-(2,2-dimethyl-4-[(di-tert-butyl phosphonoxy)dideuteromethyl]-3-oxo-5-pyrido[1,4]oxazin-6-yl)-5-fluoro-N₂-(3,4,5-trimethoxyphenyl)-2,4-pyrimidinediamine
• CAS No.: 1260832-90-3
• Molecular Formula: C₃₁H₄₂FN₆O₉P
• Molecular Weight: 694.666

Synonyms:N₄-(2,2-dimethyl-4-[(di-tert-butyl phosphonoxy)dideuteromethyl]-3-oxo-5-pyrido[1,4]oxazin-6-yl)-5-fluoro-N₂-(3,4,5-trimethoxyphenyl)-2,4-pyrimidinediamine

Chemical Property of N₄-(2,2-dimethyl-4-[(di-tert-butyl phosphonoxy)dideuteromethyl]-3-oxo-5-pyrido[1,4]oxazin-6-yl)-5-fluoro-N₂-(3,4,5-trimethoxyphenyl)-2,4-pyrimidinediamine

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Technology Process of N₄-(2,2-dimethyl-4-[(di-tert-butyl phosphonoxy)dideuteromethyl]-3-oxo-5-pyrido[1,4]oxazin-6-yl)-5-fluoro-N₂-(3,4,5-trimethoxyphenyl)-2,4-pyrimidinediamine

There total 1 articles about N₄-(2,2-dimethyl-4-[(di-tert-butyl phosphonoxy)dideuteromethyl]-3-oxo-5-pyrido[1,4]oxazin-6-yl)-5-fluoro-N₂-(3,4,5-trimethoxyphenyl)-2,4-pyrimidinediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-[[5-fluoro-2-(3,4,5-trimethoxyanilino)pyrimidin-4-yl]amino]-2,2-dimethyl-4H-pyrido[3,2-b][1,4]oxazin-3-one (841290-80-0) + di-tert-butyl chlorodideuteromethyl phosphate (1260832-82-3) → C31H40(2)H2FN6O9P + N4-(2,2-dimethyl-4-[(di-tert-butyl phosphonoxy)dideuteromethyl]-3-oxo-5-pyrido[1,4]oxazin-6-yl)-5-fluoro-N2-(3,4,5-trimethoxyphenyl)-2,4-pyrimidinediamine (1260832-90-3)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

Reference yield:

N4-(2,2-dimethyl-4-[(di-tert-butyl phosphonoxy)dideuteromethyl]-3-oxo-5-pyrido[1,4]oxazin-6-yl)-5-fluoro-N2-(3,4,5-trimethoxyphenyl)-2,4-pyrimidinediamine (1260832-90-3) → N4-(2,2-dimethyl-4-[(dihydrogen phosphonoxy)dideuteromethyl]-3-oxo-5-pyrido[1,4]oxazin-6-yl)-5-fluoro-N2-(3,4,5-trimethoxyphenyl)-2,4-pyrimidinediamine (1260832-74-3)

Guidance literature:

With acetic acid; In water; at 60 ℃; for 1h;

upstream raw materials:

6-[[5-fluoro-2-(3,4,5-trimethoxyanilino)pyrimidin-4-yl]amino]-2,2-dimethyl-4H-pyrido[3,2-b][1,4]oxazin-3-one

di-tert-butyl chlorodideuteromethyl phosphate

Downstream raw materials:

N₄-(2,2-dimethyl-4-[(dihydrogen phosphonoxy)dideuteromethyl]-3-oxo-5-pyrido[1,4]oxazin-6-yl)-5-fluoro-N₂-(3,4,5-trimethoxyphenyl)-2,4-pyrimidinediamine

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