C₂HF₃O₂*C₃₆H₄₀N₆O₆

Base Information

Chemical Name:C₂HF₃O₂*C₃₆H₄₀N₆O₆
CAS No.:1262657-49-7
Molecular Formula:C₂HF₃O₂*C₃₆H₄₀N₆O₆
Molecular Weight:766.774
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>36</sub>H<sub>40</sub>N<sub>6</sub>O<sub>6</sub>

Synonyms:C₂HF₃O₂*C₃₆H₄₀N₆O₆

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Chemical Property of C₂HF₃O₂*C₃₆H₄₀N₆O₆

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Technology Process of C₂HF₃O₂*C₃₆H₄₀N₆O₆

There total 17 articles about C₂HF₃O₂*C₃₆H₄₀N₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1262657-45-3
C₃₆H₃₈N₈O₆

: 76-05-1
trifluoroacetic acid

: 1262657-49-7
C₂HF₃O₂*C₃₆H₄₀N₆O₆

Guidance literature:: C₃₆H₃₈N₈O₆; With triphenylphosphine; In tetrahydrofuran; water; at 80 ℃; for 1h;

trifluoroacetic acid; In tetrahydrofuran; water; at 23 ℃;
DOI:10.1039/c0cc02214d

Reference yield:

: C₁₉H₂₀N₂O₃

: 1262657-49-7
C₂HF₃O₂*C₃₆H₄₀N₆O₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: trichlorophosphate / mineral oil / 2 h / 0 - 23 °C / Inert atmosphere

1.2: 1 h / 23 °C / Cooling with ice

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C

2.2: 2 h / -78 °C

3.1: Dess-Martin periodane / dichloromethane; water / 2 h / 23 °C

4.1: manganese(III) triacetate dihydrate; acetic acid / 0 - 60 °C / Inert atmosphere

5.1: lithium hydroxide / tetrahydrofuran; water / 0.5 h / 23 °C

5.2: 0 - 23 °C / Inert atmosphere

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 - 0 °C

7.1: calcium borohydride bis(tetrahydrofuran) / tetrahydrofuran / 0.5 h / 0 - 23 °C

7.2: 0.5 h / 0 - 50 °C

8.1: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

9.1: water; Dess-Martin periodane / dichloromethane / 0.25 h / 40 °C

10.1: hydrogenchloride / methanol; water / 2 h / 0 - 40 °C

11.1: potassium hydrogen phthalate / methanol; water / 10 - 15 °C / pH 3.7

11.2: 110 °C

12.1: triphenylphosphine / tetrahydrofuran; water / 1 h / 80 °C

12.2: 23 °C

With hydrogenchloride; calcium borohydride bis(tetrahydrofuran); water; potassium hydrogen phthalate; manganese(III) triacetate dihydrate; Dess-Martin periodane; acetic acid; triphenylphosphine; trifluoroacetic acid; lithium hydroxide; lithium hexamethyldisilazane; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; water; mineral oil; 5.2: Mitsunobu reaction / 12.1: Staudinger reaction;
DOI:10.1039/c0cc02214d

Reference yield:

: C₄₄H₅₄N₄O₁₁

: 1262657-49-7
C₂HF₃O₂*C₃₆H₄₀N₆O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: Dess-Martin periodane / dichloromethane; water / 2 h / 23 °C

2.1: manganese(III) triacetate dihydrate; acetic acid / 0 - 60 °C / Inert atmosphere

3.1: lithium hydroxide / tetrahydrofuran; water / 0.5 h / 23 °C

3.2: 0 - 23 °C / Inert atmosphere

4.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 - 0 °C

5.1: calcium borohydride bis(tetrahydrofuran) / tetrahydrofuran / 0.5 h / 0 - 23 °C

5.2: 0.5 h / 0 - 50 °C

6.1: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

7.1: water; Dess-Martin periodane / dichloromethane / 0.25 h / 40 °C

8.1: hydrogenchloride / methanol; water / 2 h / 0 - 40 °C

9.1: potassium hydrogen phthalate / methanol; water / 10 - 15 °C / pH 3.7

9.2: 110 °C

10.1: triphenylphosphine / tetrahydrofuran; water / 1 h / 80 °C

10.2: 23 °C

With hydrogenchloride; calcium borohydride bis(tetrahydrofuran); water; potassium hydrogen phthalate; manganese(III) triacetate dihydrate; Dess-Martin periodane; acetic acid; triphenylphosphine; trifluoroacetic acid; lithium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; water; 3.2: Mitsunobu reaction / 10.1: Staudinger reaction;
DOI:10.1039/c0cc02214d