C₃₃H₄₃NO₉Si

Base Information

Chemical Name:C₃₃H₄₃NO₉Si
CAS No.:1280608-61-8
Molecular Formula:C₃₃H₄₃NO₉Si
Molecular Weight:625.791
Hs Code.:

C<sub>33</sub>H<sub>43</sub>NO<sub>9</sub>Si

Synonyms:C₃₃H₄₃NO₉Si

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Chemical Property of C₃₃H₄₃NO₉Si

Chemical Property:

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Technology Process of C₃₃H₄₃NO₉Si

There total 8 articles about C₃₃H₄₃NO₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1280608-60-7
C₃₆H₅₁NO₉Si₂

: 1280608-61-8
C₃₃H₄₃NO₉Si

Guidance literature:: With pyridine; pyridine hydrofluoride; In tetrahydrofuran; at -78 - 0 ℃; for 8h;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-50-5
C₂₃H₂₇NO₆

: 1280608-61-8
C₃₃H₄₃NO₉Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

1.2: 2.5 h / 20 °C

2.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

3.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

4.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

5.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

6.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 8 h / -78 - 0 °C

With pyridine; 2,6-dimethylpyridine; Oxone; C₁₃H₂₀O₉; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; Dimethoxymethane; dichloromethane; water; acetonitrile; mineral oil; 2.1: Shi epoxidation;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-40-3
C₂₃H₂₅NO₆

: 1280608-61-8
C₃₃H₄₃NO₉Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

2.2: 2.5 h / 20 °C

3.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

4.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

5.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

6.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

7.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 8 h / -78 - 0 °C

With pyridine; 2,6-dimethylpyridine; Oxone; sodium tetrahydroborate; C₁₃H₂₀O₉; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; Dimethoxymethane; dichloromethane; water; acetonitrile; mineral oil; 3.1: Shi epoxidation;
DOI:10.1002/anie.201006528