5-(4-HYDROXYPHENYL)-8,8-DIMETHYL-5,8,9,10-TETRAHYDROPYRIMIDO[4,5-B]QUINOLINE-2,4,6(1H,3H,7H)-TRIONE

Base Information

Chemical Name:5-(4-HYDROXYPHENYL)-8,8-DIMETHYL-5,8,9,10-TETRAHYDROPYRIMIDO[4,5-B]QUINOLINE-2,4,6(1H,3H,7H)-TRIONE
CAS No.:304661-89-0
Molecular Formula:C₁₉H₁₉N₃O₄
Molecular Weight:353.378
Hs Code.:
Mol file:304661-89-0.mol

Synonyms:5-(4-hydroxyphenyl)-8,8-dimethyl-8,9-dihydropyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)-trione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(4-HYDROXYPHENYL)-8,8-DIMETHYL-5,8,9,10-TETRAHYDROPYRIMIDO[4,5-B]QUINOLINE-2,4,6(1H,3H,7H)-TRIONE

Chemical Property:

Melting Point:>300 °C
PKA:9.50±0.60(Predicted)
Density:1.44±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of 5-(4-HYDROXYPHENYL)-8,8-DIMETHYL-5,8,9,10-TETRAHYDROPYRIMIDO[4,5-B]QUINOLINE-2,4,6(1H,3H,7H)-TRIONE

There total 2 articles about 5-(4-HYDROXYPHENYL)-8,8-DIMETHYL-5,8,9,10-TETRAHYDROPYRIMIDO[4,5-B]QUINOLINE-2,4,6(1H,3H,7H)-TRIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 873-83-6
4-Amino-2,6-dihydroxypyrimidine

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 126-81-8
dimedone

: 304661-89-0
5-(4-hydroxyphenyl)-8,8-dimethyl-8,9-dihydropyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)-trione

Guidance literature:: With N-benzyl-N,N,N-triethylammonium chloride; In water; at 90 ℃; for 22h;
DOI:10.1002/jhet.57

Reference yield: 94.0%

: 67-52-7,944357-77-1
BARBITURIC ACID

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 126-81-8
dimedone

: 304661-89-0
5-(4-hydroxyphenyl)-8,8-dimethyl-8,9-dihydropyrimido[4,5-b]quinoline-2,4,6(1H,3H,5H,7H,10H)-trione

Guidance literature:: BARBITURIC ACID; 4-hydroxy-benzaldehyde; dimedone; In ethanol; for 0.0166667h; Sonication; Green chemistry;

With ammonium acetate; In ethanol; for 0.0833333h; Sonication; Green chemistry;
DOI:10.1002/aoc.4996