Technology Process of C40H39N3O4S3
There total 6 articles about C40H39N3O4S3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diisobutylaluminium hydride / toluene / 1 h / 0 °C
2.1: N-ethyl-N,N-diisopropylamine; titanium tetrachloride / dichloromethane / 1.08 h / -78 °C
2.2: 1 h / -78 °C
3.1: dmap / dichloromethane / 2 h / 25 °C
With
dmap; titanium tetrachloride; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; toluene;
DOI:10.1016/j.bmcl.2014.07.006
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / dichloromethane / 0.5 h / 0 °C
2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 16 h / 0 - 25 °C
3.1: diisobutylaluminium hydride / toluene / 1 h / 0 °C
4.1: N-ethyl-N,N-diisopropylamine; titanium tetrachloride / dichloromethane / 1.08 h / -78 °C
4.2: 1 h / -78 °C
5.1: dmap / dichloromethane / 2 h / 25 °C
With
dmap; titanium tetrachloride; sodium hydride; diisobutylaluminium hydride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1016/j.bmcl.2014.07.006