3-((tert-butyldimethylsilyl)ethynyl)-9-hydroxy-2-((methoxymethoxy)methyl)-1,4-anthraquinone

Base Information

Chemical Name:3-((tert-butyldimethylsilyl)ethynyl)-9-hydroxy-2-((methoxymethoxy)methyl)-1,4-anthraquinone
CAS No.:1239333-72-2
Molecular Formula:C₂₅H₂₈O₅Si
Molecular Weight:436.58
Hs Code.:

Synonyms:3-((tert-butyldimethylsilyl)ethynyl)-9-hydroxy-2-((methoxymethoxy)methyl)-1,4-anthraquinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-((tert-butyldimethylsilyl)ethynyl)-9-hydroxy-2-((methoxymethoxy)methyl)-1,4-anthraquinone

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Technology Process of 3-((tert-butyldimethylsilyl)ethynyl)-9-hydroxy-2-((methoxymethoxy)methyl)-1,4-anthraquinone

There total 1 articles about 3-((tert-butyldimethylsilyl)ethynyl)-9-hydroxy-2-((methoxymethoxy)methyl)-1,4-anthraquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1239333-69-7
C₁₇H₂₃ClO₄Si

: 703-59-3
homophthalic anhydride

: 1239333-75-5
3-((tert-butyldimethylsilyl)ethynyl)-1-chloro-2,5-dihydroxy-4-((methoxymethoxy)-methyl)benzene

: 1239333-72-2
3-((tert-butyldimethylsilyl)ethynyl)-9-hydroxy-2-((methoxymethoxy)methyl)-1,4-anthraquinone

Guidance literature:: homophthalic anhydride; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere;

C₁₇H₂₃ClO₄Si; In tetrahydrofuran; hexane; at 20 ℃; for 0.0833333h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; hexane; at 0 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo100913s