1,1-dimethylethyl 4-[5-(phenylsulfonyl)-2,3-dihydro-1H-indol-1-yl]-1-piperidinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl 4-[5-(phenylsulfonyl)-2,3-dihydro-1H-indol-1-yl]-1-piperidinecarboxylate
CAS No.:882669-57-0
Molecular Formula:C₂₄H₃₀N₂O₄S
Molecular Weight:442.579
Hs Code.:

Synonyms:1,1-dimethylethyl 4-[5-(phenylsulfonyl)-2,3-dihydro-1H-indol-1-yl]-1-piperidinecarboxylate

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Chemical Property of 1,1-dimethylethyl 4-[5-(phenylsulfonyl)-2,3-dihydro-1H-indol-1-yl]-1-piperidinecarboxylate

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Technology Process of 1,1-dimethylethyl 4-[5-(phenylsulfonyl)-2,3-dihydro-1H-indol-1-yl]-1-piperidinecarboxylate

There total 2 articles about 1,1-dimethylethyl 4-[5-(phenylsulfonyl)-2,3-dihydro-1H-indol-1-yl]-1-piperidinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 368-43-4
phenylsulfonyl fluoride

: 882669-57-0
1,1-dimethylethyl 4-[5-(phenylsulfonyl)-2,3-dihydro-1H-indol-1-yl]-1-piperidinecarboxylate

Guidance literature:: tert-butyl 4-(5-bromoindolin-1-yl)piperidine-1-carboxylate; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 - -60 ℃; for 0.0833333h;

phenylsulfonyl fluoride; In tetrahydrofuran; pentane; at -70 - 20 ℃; for 1.25h; Product distribution / selectivity;

Reference yield: 28.0%

: 401565-86-4
tert-butyl 4-(5-bromoindolin-1-yl)piperidine-1-carboxylate

: 873-55-2
sodium benzenesulfonate

: 882669-57-0
1,1-dimethylethyl 4-[5-(phenylsulfonyl)-2,3-dihydro-1H-indol-1-yl]-1-piperidinecarboxylate

Guidance literature:: With potassium carbonate; copper(l) iodide; N,N`-dimethylethylenediamine; In dimethyl sulfoxide; at 100 ℃; for 18h; Product distribution / selectivity;

Reference yield: 94.0%

: 882669-57-0
1,1-dimethylethyl 4-[5-(phenylsulfonyl)-2,3-dihydro-1H-indol-1-yl]-1-piperidinecarboxylate

: 882669-55-8
1,1-dimethylethyl 4-[5-(phenylsulfonyl)-1H-indol-1-yl]-1-piperidinecarboxylate

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; at 0 - 20 ℃; for 5h; Product distribution / selectivity;