dichloro-2,4 trimethoxy-1,3,5 benzene

Base Information

• Chemical Name: dichloro-2,4 trimethoxy-1,3,5 benzene
• CAS No.: 77440-84-7
• Molecular Formula: C₉H₁₀Cl₂O₃
• Molecular Weight: 237.083
• Mol file: 77440-84-7.mol

Synonyms:dichloro-2,4 trimethoxy-1,3,5 benzene

Chemical Property of dichloro-2,4 trimethoxy-1,3,5 benzene

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dichloro-2,4 trimethoxy-1,3,5 benzene

There total 5 articles about dichloro-2,4 trimethoxy-1,3,5 benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1,2,3-trimethoxybenzene (621-23-8) → dichloro-2,4 trimethoxy-1,3,5 benzene (77440-84-7)

Guidance literature:

With benzyltrimethylazanium tetrachloro-λ³-iodanuide; In acetic acid; for 1h; Ambient temperature;

DOI:10.1246/cl.1989.415

Reference yield: 88.0%

1,2,3-trimethoxybenzene (621-23-8) → 2,4,6-trimethoxychlorobenzene (67827-56-9) + dichloro-2,4 trimethoxy-1,3,5 benzene (77440-84-7)

Guidance literature:

With dihydrogen peroxide; acetic acid; lithium chloride; In water; 1,2-dichloro-ethane; at 60 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c0cc04889e

Reference yield:

2,4,6-trimethoxybenzoic acid (570-02-5) → 1,2,3-trimethoxybenzene (621-23-8) + 2,4,6-trimethoxychlorobenzene (67827-56-9) + dichloro-2,4 trimethoxy-1,3,5 benzene (77440-84-7)

Guidance literature:

With sodium persulfate; N-chloro-succinimide; ethanol; at 60 ℃; for 18h; Sealed tube;

DOI:10.1016/j.tetlet.2017.10.036

upstream raw materials:

1,2,3-trimethoxybenzene

1-(2,4,6-trimethoxyphenyl)ethanone

2,4,6-trimethoxybenzoic acid

Downstream raw materials:

2,6-dichloro-3,5-dimethoxycyclohexa-2,5-diene-1,4-dione

1,3,5-trichloro-2,4,6-trimethoxybenzene

3-acetoxy-2,4-dichloro-1,5-dimethoxy-benzene