(R,E)-3-(4-(4-methoxybenzyloxy)-3-(triisopropylsilyloxy)butylidene)dihydrofuran-2(3H)-one

Base Information

Chemical Name:(R,E)-3-(4-(4-methoxybenzyloxy)-3-(triisopropylsilyloxy)butylidene)dihydrofuran-2(3H)-one
CAS No.:1164114-92-4
Molecular Formula:C₂₅H₄₀O₅Si
Molecular Weight:448.675
Hs Code.:

Synonyms:(R,E)-3-(4-(4-methoxybenzyloxy)-3-(triisopropylsilyloxy)butylidene)dihydrofuran-2(3H)-one

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Chemical Property of (R,E)-3-(4-(4-methoxybenzyloxy)-3-(triisopropylsilyloxy)butylidene)dihydrofuran-2(3H)-one

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Technology Process of (R,E)-3-(4-(4-methoxybenzyloxy)-3-(triisopropylsilyloxy)butylidene)dihydrofuran-2(3H)-one

There total 1 articles about (R,E)-3-(4-(4-methoxybenzyloxy)-3-(triisopropylsilyloxy)butylidene)dihydrofuran-2(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 34932-07-5
3-(triphenylphosphoranyliden)dihydro-2(3H)-furanone

: 1164114-91-3
(R)-4-(4-methoxybenzyloxy)-3-(triisopropylsilyloxy)butanal

: 1164114-92-4
(R,E)-3-(4-(4-methoxybenzyloxy)-3-(triisopropylsilyloxy)butylidene)dihydrofuran-2(3H)-one

Guidance literature:: In tetrahydrofuran; at 50 ℃; Inert atmosphere;
DOI:10.1021/ol900757k

Reference yield: 99.0%

: 1164114-92-4
(R,E)-3-(4-(4-methoxybenzyloxy)-3-(triisopropylsilyloxy)butylidene)dihydrofuran-2(3H)-one

: 1164115-07-4
(2E,5R)-2-(2'-hydroxyethyl)-6-(p-methoxybenzyloxy)-5-(tri-isopropylsilanyloxy)-hex-2-enoic acid

Guidance literature:: With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1021/ol900757k

Reference yield:

: 1164114-92-4
(R,E)-3-(4-(4-methoxybenzyloxy)-3-(triisopropylsilyloxy)butylidene)dihydrofuran-2(3H)-one

: C₂₅H₄₂O₇Si

: 1234579-83-9
C₂₅H₄₂O₇Si

Guidance literature:: With potassium osmate(VI) dihydrate; methanesulfonamide; water; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); In tert-butyl alcohol; at 0 ℃; for 15h; optical yield given as %de;
DOI:10.1002/chem.201000104