9-(4-chlorophenyl)-3,3-dimethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione

Base Information

Chemical Name:9-(4-chlorophenyl)-3,3-dimethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione
CAS No.:1609076-76-7
Molecular Formula:C₂₁H₂₁ClO₃
Molecular Weight:356.849
Hs Code.:

Synonyms:9-(4-chlorophenyl)-3,3-dimethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione

Suppliers and Price of 9-(4-chlorophenyl)-3,3-dimethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione

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Chemical Property of 9-(4-chlorophenyl)-3,3-dimethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione

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Technology Process of 9-(4-chlorophenyl)-3,3-dimethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione

There total 4 articles about 9-(4-chlorophenyl)-3,3-dimethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1609076-47-2
2-[(4-chlorophenyl)(phenylthio)methyl]-3-hydroxy-5,5-dimethylcyclohex-2-enone

: 504-02-9
1,3-cylohexanedione

: 1609076-76-7
9-(4-chlorophenyl)-3,3-dimethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione

Guidance literature:: With acetic acid; at 100 ℃; for 8h;
DOI:10.1002/adsc.201300790

Reference yield: 80.0%

: 104-88-1
4-chlorobenzaldehyde

: 504-02-9
1,3-cylohexanedione

: 126-81-8
dimedone

: 1609076-76-7
9-(4-chlorophenyl)-3,3-dimethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione

: 15782-02-2
9-(4-chlorophenyl)-3,3,6,6-tetramethyl-2,3,4,5,6,7,8,9-octahydroxanthene-1,8-dione

Guidance literature:: With ascorbic acid; In ethanol; for 6h; regioselective reaction; Reflux;
DOI:10.1016/j.tetlet.2014.08.040

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1609076-76-7
9-(4-chlorophenyl)-3,3-dimethyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8(2H)-dione

Guidance literature:: Multi-step reaction with 2 steps

1: L-proline / ethanol / 6 h / 30 °C

2: acetic acid / 8 h / 100 °C

With acetic acid; L-proline; In ethanol;
DOI:10.1002/adsc.201300790