methyl 3-cyclopropyl-2-(3-(2,2,2-trifluoroethoxy)-5-(trifluoromethylsulfonyloxy)phenyl)propanoate

Base Information

• Chemical Name: methyl 3-cyclopropyl-2-(3-(2,2,2-trifluoroethoxy)-5-(trifluoromethylsulfonyloxy)phenyl)propanoate
• CAS No.: 1155807-88-7
• Molecular Formula: C₁₆H₁₆F₆O₆S
• Molecular Weight: 450.356

Synonyms:methyl 3-cyclopropyl-2-(3-(2,2,2-trifluoroethoxy)-5-(trifluoromethylsulfonyloxy)phenyl)propanoate

Chemical Property of methyl 3-cyclopropyl-2-(3-(2,2,2-trifluoroethoxy)-5-(trifluoromethylsulfonyloxy)phenyl)propanoate

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Technology Process of methyl 3-cyclopropyl-2-(3-(2,2,2-trifluoroethoxy)-5-(trifluoromethylsulfonyloxy)phenyl)propanoate

There total 1 articles about methyl 3-cyclopropyl-2-(3-(2,2,2-trifluoroethoxy)-5-(trifluoromethylsulfonyloxy)phenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trifluoromethylsulfonic anhydride (358-23-6) + methyl 3-cyclopropyl-2-(3-hydroxy-5-(2,2,2-trifluoroethoxy)phenyl)propanoate (1155807-84-3) → methyl 3-cyclopropyl-2-(3-(2,2,2-trifluoroethoxy)-5-(trifluoromethylsulfonyloxy)phenyl)propanoate (1155807-88-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.5h; Product distribution / selectivity;

Reference yield:

methyl 3-cyclopropyl-2-(3-(2,2,2-trifluoroethoxy)-5-(trifluoromethylsulfonyloxy)phenyl)propanoate (1155807-88-7) + benzo[c][1,2,5]oxadiazole-5-boronic acid (426268-09-9) → methyl 2-(3-(benzo[c][1,2,5]oxadiazol-5-yl)-5-(2,2,2-trifluoroethoxy)phenyl)-3-cyclopropylpropanoate (1155807-86-5)

Guidance literature:

With caesium carbonate; palladium(II); In 1,4-dioxane; at 100 ℃; for 3h;

Reference yield:

benzo[c][1,2,5]thiadiazol-5-ylboronic acid (191341-04-5) + methyl 3-cyclopropyl-2-(3-(2,2,2-trifluoroethoxy)-5-(trifluoromethylsulfonyloxy)phenyl)propanoate (1155807-88-7) → methyl 2-(3-(benzo[c][1,2,5]thiadiazol-5-yl)-5-(2,2,2-trifluoroethoxy)phenyl)-3-cyclopropylpropanoate (1155807-90-1)

Guidance literature:

With caesium carbonate; palladium(II); In 1,4-dioxane; at 100 ℃; for 3h;

upstream raw materials:

trifluoromethylsulfonic anhydride

methyl 3-cyclopropyl-2-(3-hydroxy-5-(2,2,2-trifluoroethoxy)phenyl)propanoate

Downstream raw materials:

methyl 2-(3-(benzo[c][1,2,5]oxadiazol-5-yl)-5-(2,2,2-trifluoroethoxy)phenyl)-3-cyclopropylpropanoate

methyl 2-(3-(benzo[c][1,2,5]thiadiazol-5-yl)-5-(2,2,2-trifluoroethoxy)phenyl)-3-cyclopropylpropanoate

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