triethylammonium S-phenyl 3'-O-dianilinophosphinyl-5'-O-methyl>-6-N-benzoyladenosine 2'-phosphorothioate

Base Information

• Chemical Name: triethylammonium S-phenyl 3'-O-dianilinophosphinyl-5'-O-methyl>-6-N-benzoyladenosine 2'-phosphorothioate
• CAS No.: 97997-70-1
• Molecular Formula: C₆H₁₅N*C₇₈H₅₀Cl₆N₁₀O₁₄P₂S
• Molecular Weight: 1759.24

Synonyms:triethylammonium S-phenyl 3'-O-dianilinophosphinyl-5'-O-methyl>-6-N-benzoyladenosine 2'-phosphorothioate

Chemical Property of triethylammonium S-phenyl 3'-O-dianilinophosphinyl-5'-O-methyl>-6-N-benzoyladenosine 2'-phosphorothioate

Chemical Property:

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Technology Process of triethylammonium S-phenyl 3'-O-dianilinophosphinyl-5'-O-methyl>-6-N-benzoyladenosine 2'-phosphorothioate

There total 2 articles about triethylammonium S-phenyl 3'-O-dianilinophosphinyl-5'-O-methyl>-6-N-benzoyladenosine 2'-phosphorothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate (97997-68-7) + pyridinium phosphinate → triethylammonium S-phenyl 3'-O-dianilinophosphinyl-5'-O-methyl>-6-N-benzoyladenosine 2'-phosphorothioate (97997-70-1)

Guidance literature:

In pyridine; for 1h; Yield given; Ambient temperature;

DOI:10.1021/ja00306a046

Reference yield:

triethylamine carbonate (15715-58-9) + 2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate (97997-68-7) → triethylammonium S-phenyl 3'-O-dianilinophosphinyl-5'-O-methyl>-6-N-benzoyladenosine 2'-phosphorothioate (97997-70-1)

Guidance literature:

With H₂O₂P*C₅H₅N; Multistep reaction; 1) pyridine, room. temp., 1h, 2) CH₂Cl₂;

DOI:10.1246/bcsj.64.588

Reference yield: 92.0%

triethylammonium S-phenyl 3'-O-dianilinophosphinyl-5'-O-methyl>-6-N-benzoyladenosine 2'-phosphorothioate (97997-70-1) + 2',3'-O-(methoxymethylene)-O6-(diphenylcarbamoyl)-N2-propionylguanosine (97997-71-2) → C106H76Cl6N16O21P2S

Guidance literature:

With 3-nitro-1,2,4-tetrazole; 2,4,5,6-tetramethylbenzenedisulfonyl dichloride; In pyridine; for 2h; Ambient temperature;

DOI:10.1021/ja00306a046

upstream raw materials:

triethylamine carbonate

2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate

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