4H,8H-Benzo<1,2-c:4,5-c'>bis<1,2,5>thiadiazol-4,8-dion-di-p-tosylhydrazon

Base Information

Chemical Name:4H,8H-Benzo<1,2-c:4,5-c'>bis<1,2,5>thiadiazol-4,8-dion-di-p-tosylhydrazon
CAS No.:83274-19-5
Molecular Formula:C₂₀H₁₆N₈O₄S₄
Molecular Weight:560.662
Hs Code.:

Synonyms:4H,8H-Benzo<1,2-c:4,5-c'>bis<1,2,5>thiadiazol-4,8-dion-di-p-tosylhydrazon

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4H,8H-Benzo<1,2-c:4,5-c'>bis<1,2,5>thiadiazol-4,8-dion-di-p-tosylhydrazon

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Technology Process of 4H,8H-Benzo<1,2-c:4,5-c'>bis<1,2,5>thiadiazol-4,8-dion-di-p-tosylhydrazon

There total 2 articles about 4H,8H-Benzo<1,2-c:4,5-c'>bis<1,2,5>thiadiazol-4,8-dion-di-p-tosylhydrazon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 83274-15-1,91120-84-2
4H,8H-benzo<1,2-c;4,5-c'>bis<1,2,5>thiadiazole-4,8-dione

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 83274-19-5
4H,8H-Benzo<1,2-c:4,5-c'>bis<1,2,5>thiadiazol-4,8-dion-di-p-tosylhydrazon

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; methanol; Heating;

Reference yield:

: 1128-13-8
2,3,5,6-tetraaminocyclohexa-2,5-diene-1,4-dione

: 83274-19-5
4H,8H-Benzo<1,2-c:4,5-c'>bis<1,2,5>thiadiazol-4,8-dion-di-p-tosylhydrazon

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / SOCl₂

2: 98 percent / HCl / methanol; tetrahydrofuran / Heating

With hydrogenchloride; thionyl chloride; In tetrahydrofuran; methanol;