N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(4-dimethylaminophenylamino)-ethylamine

Base Information

Chemical Name:N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(4-dimethylaminophenylamino)-ethylamine
CAS No.:102246-97-9
Molecular Formula:C₂₅H₃₆N₄O₃
Molecular Weight:440.586
Hs Code.:

Synonyms:N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(4-dimethylaminophenylamino)-ethylamine

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Chemical Property of N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(4-dimethylaminophenylamino)-ethylamine

Chemical Property:

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Technology Process of N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(4-dimethylaminophenylamino)-ethylamine

There total 5 articles about N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(4-dimethylaminophenylamino)-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 85175-65-1
7,8-dimethoxy-3-(3-chloropropyl)-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one

: N-(p-dimethylaminophenyl)ethylenediamine

: 102246-97-9
N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(4-dimethylaminophenylamino)-ethylamine

Guidance literature:

Reference yield:

: 10313-60-7
3,4-dimethoxyphenylacetyl chloride

: 102246-97-9
N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(4-dimethylaminophenylamino)-ethylamine

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / dichloromethane

2: hydrogenchloride; acetic acid

3: potassium tert-butylate / dimethyl sulfoxide; acetone

4: palladium/charcoal; water; acetic acid

With potassium tert-butylate; triethylamine; In hydrogenchloride; palladium/charcoal; dichloromethane; water; acetic acid; dimethyl sulfoxide; acetone;

Reference yield:

: 73942-87-7
7,8-Dimethoxy-1,3-dihydro-2H-3-benzazepin-2-one

: 102246-97-9
N-[3-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-propyl]-2-(4-dimethylaminophenylamino)-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium tert-butylate / dimethyl sulfoxide; acetone

2: palladium/charcoal; water; acetic acid

With potassium tert-butylate; In palladium/charcoal; water; acetic acid; dimethyl sulfoxide; acetone;