Boc-Phe-Ala-ψ-Ala-OBzl

Base Information

Chemical Name:Boc-Phe-Ala-ψ-Ala-OBzl
CAS No.:137234-21-0
Molecular Formula:C₂₇H₃₄N₆O₅
Molecular Weight:522.604
Hs Code.:

Synonyms:Boc-Phe-Ala-ψ-Ala-OBzl

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Chemical Property of Boc-Phe-Ala-ψ-Ala-OBzl

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Technology Process of Boc-Phe-Ala-ψ-Ala-OBzl

There total 2 articles about Boc-Phe-Ala-ψ-Ala-OBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.6%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 137234-24-3
HBr*L-Ala-ψ-L-Ala-OBzl

: 137234-21-0
Boc-Phe-Ala-ψ-Ala-OBzl

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In dichloromethane; N,N-dimethyl-formamide; a) -10 deg C, 1 h, b) r.t., overnight;
DOI:10.1021/jo00027a038

Reference yield:

: 133641-24-4
Z-L-Ala-ψ-L-Ala-OBzl

: 137234-21-0
Boc-Phe-Ala-ψ-Ala-OBzl

Guidance literature:: Multi-step reaction with 2 steps

1: 96.3 percent / 30percent HBr / acetic acid / 0.33 h / Ambient temperature

2: 66.6 percent / isobutylchloroformate, N-methylmorpholine / CH₂Cl₂; dimethylformamide / a) -10 deg C, 1 h, b) r.t., overnight

With 4-methyl-morpholine; hydrogen bromide; isobutyl chloroformate; In dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jo00027a038