(S)-N-(1-(diphenylphosphino)-3,3-dimethylbutan-2-yl)-3,5-bis(trifluoromethyl)benzamide

Base Information

• Chemical Name: (S)-N-(1-(diphenylphosphino)-3,3-dimethylbutan-2-yl)-3,5-bis(trifluoromethyl)benzamide
• CAS No.: 1239020-07-5
• Molecular Formula: C₂₇H₂₆F₆NOP
• Molecular Weight: 525.474

Synonyms:(S)-N-(1-(diphenylphosphino)-3,3-dimethylbutan-2-yl)-3,5-bis(trifluoromethyl)benzamide

Chemical Property of (S)-N-(1-(diphenylphosphino)-3,3-dimethylbutan-2-yl)-3,5-bis(trifluoromethyl)benzamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-N-(1-(diphenylphosphino)-3,3-dimethylbutan-2-yl)-3,5-bis(trifluoromethyl)benzamide

There total 1 articles about (S)-N-(1-(diphenylphosphino)-3,3-dimethylbutan-2-yl)-3,5-bis(trifluoromethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

3,5-bistrifluoromethylbenzoic acid (725-89-3) + (S)‐1‐(diphenylphosphino)‐3,3‐dimethylbutan‐2‐amine (286454-86-2,1366384-12-4) → (S)-N-(1-(diphenylphosphino)-3,3-dimethylbutan-2-yl)-3,5-bis(trifluoromethyl)benzamide (1239020-07-5)

Guidance literature:

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1002/anie.201000446

Reference yield: 94.0%

(S)-N-(1-(diphenylphosphino)-3,3-dimethylbutan-2-yl)-3,5-bis(trifluoromethyl)benzamide (1239020-07-5) + p-Methoxybenzyl bromide (2746-25-0) → (S)-(2-(3,5-bis(trifluoromethyl)benzamido)-3,3-dimethylbutyl)(4-methoxybenzyl)diphenylphosphonium bromide

Guidance literature:

In toluene; at 110 ℃; for 8h;

DOI:10.1016/j.tet.2015.02.001

Reference yield: 94.0%

(S)-N-(1-(diphenylphosphino)-3,3-dimethylbutan-2-yl)-3,5-bis(trifluoromethyl)benzamide (1239020-07-5) + 3,5-bis(trifluoromethyl)benzyl bromide (32247-96-4) → (S)-(2-(3,5-bis(trifluoromethyl)benzamido)-3,3-dimethylbutyl)(3,5-bis(trifluoromethyl)benzyl)diphenylphosphonium bromide

Guidance literature:

In toluene; at 110 ℃; for 8h;

DOI:10.1016/j.tet.2015.02.001

upstream raw materials:

3,5-bistrifluoromethylbenzoic acid

(S)‐1‐(diphenylphosphino)‐3,3‐dimethylbutan‐2‐amine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1239020-07-5 (S)-N-(1-(diphenylphosphino)-3,3-dimethylbutan-2-yl)-3,5-bis(trifluoromethyl)benzamide

Send

Send

Metric Ton KG G Pound L ML

Send

Send