1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-β-D-ribofuranose

Base Information

Chemical Name:1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-β-D-ribofuranose
CAS No.:160584-05-4
Molecular Formula:C₂₀H₂₃NO₆S
Molecular Weight:405.472
Hs Code.:

Synonyms:1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-β-D-ribofuranose

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Chemical Property of 1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-β-D-ribofuranose

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Technology Process of 1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-β-D-ribofuranose

There total 3 articles about 1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-β-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 5-O-Benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-α,β-D-ribofuranose

: C₂₂H₂₅NO₇S

: 160584-05-4
1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-β-D-ribofuranose

: 160584-04-3
1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-α-D-ribofuranose

Guidance literature:: With triethylamine; In dichloromethane; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo00100a050

Reference yield:

: 108-24-7
acetic anhydride

: 5-O-Benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-α,β-D-ribofuranose

: 160584-05-4
1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-β-D-ribofuranose

: 160584-04-3
1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-α-D-ribofuranose

Guidance literature:: With pyridine; Yield given. Yields of byproduct given;
DOI:10.1021/jo00100a050

Reference yield:

: 3034-53-5,215777-74-5
2-bromo-1,3-thiazole

: 85846-80-6
5-O-benzyl-2,3-O-isopropylidene-D-ribono-1,4-lactone

: 108-24-7
acetic anhydride

: 160584-05-4
1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-β-D-ribofuranose

: 160584-04-3
1-O-Acetyl-5-O-benzyl-2,3-O-isopropylidene-1-(2-thiazolyl)-α-D-ribofuranose

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) hexane, Et₂O, -78 deg C, 20 min; THF, -78 deg C, 20 min then -78 to -65 deg C, 30 min, 2.) -65 deg C, 1 h;
DOI:10.1021/jo00100a050