C₄₂H₆₇NO₉Si₂

Base Information Edit

Chemical Name:C₄₂H₆₇NO₉Si₂
CAS No.:1402588-81-1
Molecular Formula:C₄₂H₆₇NO₉Si₂
Molecular Weight:786.166
Hs Code.:
Mol file:1402588-81-1.mol

C<sub>42</sub>H<sub>67</sub>NO<sub>9</sub>Si<sub>2</sub>

Synonyms:C₄₂H₆₇NO₉Si₂

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Chemical Property of C₄₂H₆₇NO₉Si₂ Edit

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Technology Process of C₄₂H₆₇NO₉Si₂

There total 18 articles about C₄₂H₆₇NO₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1402588-80-0
C₅₀H₇₅NO₁₀Si₂

: 1402588-81-1
C₄₂H₆₇NO₉Si₂

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja3057612

Reference yield:

: C₁₈H₃₅NO₃Si

: 1402588-81-1
C₄₂H₆₇NO₉Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: Dess-Martin periodane / 3 h / 0 °C / Inert atmosphere

2: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; methanol / 3.5 h / -78 °C / Inert atmosphere

3: benzo[1,3,2]dioxaborole / tetrahydrofuran / 20 h / -78 - 0 °C / Inert atmosphere

4: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

5: water; ethanol / 1.33 h / Reflux

6: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; phenylborondichloride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; ethanol; dichloromethane; water;
DOI:10.1021/ja3057612

Reference yield:

: 38064-90-3
2,4-dimethoxytoluene

: 1402588-81-1
C₄₂H₆₇NO₉Si₂

Guidance literature:: Multi-step reaction with 15 steps

1: 6 h / 0 °C / Inert atmosphere

2: Inert atmosphere

3: thionyl chloride / benzene / 2 h / Reflux

4: 0 - 20 °C / Inert atmosphere

5: sec.-butyllithium / cyclohexane / 1 h / -78 °C / Inert atmosphere

6: boron tribromide / dichloromethane / 5.5 h / -78 - 25 °C / Inert atmosphere

7: dichloromethane / 20 h / 20 °C / Inert atmosphere

8: potassium carbonate / N,N-dimethyl-formamide / 20 h / 80 °C / Inert atmosphere

9: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; tert-butyl alcohol; water / 12 h / Inert atmosphere

10: sodium periodate / methanol / 1 h / 20 °C / Inert atmosphere

11: phenylborondichloride; N-ethyl-N,N-diisopropylamine / dichloromethane; methanol / 3.5 h / -78 °C / Inert atmosphere

12: benzo[1,3,2]dioxaborole / tetrahydrofuran / 20 h / -78 - 0 °C / Inert atmosphere

13: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 °C / Inert atmosphere

14: water; ethanol / 1.33 h / Reflux

15: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; thionyl chloride; phenylborondichloride; sec.-butyllithium; boron tribromide; potassium carbonate; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; ethanol; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; tert-butyl alcohol; benzene;
DOI:10.1021/ja3057612