Technology Process of C19H8Cl2F9N5
There total 6 articles about C19H8Cl2F9N5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium dithionite; sodium hydroxide;
tetrabutylammomium bromide;
In
tetrahydrofuran; water;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / triphenylphosphine; palladium diacetate / 4.25 h / 100 °C / Inert atmosphere; Reflux
2: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h / 20 °C
3: N,N-dimethyl-formamide / 24 h / 20 °C
4: sodium hydroxide; sodium dithionite / tetrabutylammomium bromide / water; tetrahydrofuran / 3 h / 20 °C
With
sodium dithionite; triethylamine; sodium hydroxide;
copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; palladium diacetate; sodium L-ascorbate; triphenylphosphine;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-chloro-succinimide / dichloromethane / 20 °C
2.1: hydrogenchloride / water / 0.5 h / 20 °C
2.2: 0.5 h / 0 - 5 °C
2.3: 0 - 20 °C
3.1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h / 20 °C
4.1: N,N-dimethyl-formamide / 24 h / 20 °C
5.1: sodium hydroxide; sodium dithionite / tetrabutylammomium bromide / water; tetrahydrofuran / 3 h / 20 °C
With
hydrogenchloride; N-chloro-succinimide; sodium dithionite; sodium hydroxide;
copper(ll) sulfate pentahydrate; tetrabutylammomium bromide; sodium L-ascorbate;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;