MIDA boryl benzoate

Base Information

Chemical Name:MIDA boryl benzoate
CAS No.:1414852-74-6
Molecular Formula:C₁₂H₁₂BNO₆
Molecular Weight:277.041
Hs Code.:

Synonyms:MIDA boryl benzoate

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Chemical Property of MIDA boryl benzoate

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Technology Process of MIDA boryl benzoate

There total 5 articles about MIDA boryl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1414852-68-8
2-benzoyl-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

: 1414852-74-6
MIDA boryl benzoate

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 23 ℃; for 1h;
DOI:10.1002/anie.201206501

Reference yield:

: (Z)-2-(1,2-diphenylprop-1-en-1-yl)-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

: 1414852-68-8
2-benzoyl-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione

: 1414852-74-6
MIDA boryl benzoate

Guidance literature:: (Z)-2-(1,2-diphenylprop-1-en-1-yl)-6-methyl-1,3,6,2-dioxazaborocane-4,8-dione; With ozone; In acetone; at -78 ℃; Sealed tube;

With dimethylsulfide; In acetone; at -78 ℃; for 0.0833333h; Overall yield = 84 %; Sealed tube;
DOI:10.1002/anie.201707933

Reference yield:

: 1329422-36-7
2-(N-methyliminodiacetylboryl)-2-phenylacetic acid

: 1414852-74-6
MIDA boryl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 23 °C / Inert atmosphere; Darkness

2.1: 2-methylpropan-2-thiol; oxygen / dichloromethane / 23 °C / Irradiation

2.2: 2 h / 23 °C

3.1: Dess-Martin periodane / dichloromethane; water / 23 °C

4.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 23 °C

With dmap; oxygen; sodium hydrogencarbonate; Dess-Martin periodane; 2-methylpropan-2-thiol; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In dichloromethane; water; 3.1: |Dess-Martin Oxidation / 4.1: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1002/anie.201206501