Technology Process of C32H34F3NOS2
There total 5 articles about C32H34F3NOS2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C38H48F3NOS2Si;
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
With
water;
In
tetrahydrofuran; ethyl acetate;
Inert atmosphere;
DOI:10.1016/j.ejmech.2012.03.055
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
1.2: 0.5 h / -78 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
3.2: 0.5 h / -78 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
4.2: Inert atmosphere
With
1H-imidazole; tetrabutyl ammonium fluoride; isopropylmagnesium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.03.055
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
1.2: 0.5 h / -78 °C
2.1: 1H-imidazole / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
3.2: 0.5 h / -78 °C / Inert atmosphere
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
4.2: Inert atmosphere
With
1H-imidazole; tetrabutyl ammonium fluoride; isopropylmagnesium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.03.055