Triphenyl<(2-tetrahydropyranyloxy)methyl>phosphonium chloride

Base Information

Chemical Name:Triphenyl<(2-tetrahydropyranyloxy)methyl>phosphonium chloride
CAS No.:56061-88-2
Molecular Formula:C₂₄H₂₆O₂P*Cl
Molecular Weight:412.896
Hs Code.:

Synonyms:Triphenyl<(2-tetrahydropyranyloxy)methyl>phosphonium chloride

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Chemical Property of Triphenyl<(2-tetrahydropyranyloxy)methyl>phosphonium chloride

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Technology Process of Triphenyl<(2-tetrahydropyranyloxy)methyl>phosphonium chloride

There total 1 articles about Triphenyl<(2-tetrahydropyranyloxy)methyl>phosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56061-88-2
Triphenyl<(2-tetrahydropyranyloxy)methyl>phosphonium chloride

Guidance literature:: Phosphin C18H15P, Dihydropyran;
DOI:10.1016/0040-4020(75)80017-2

Reference yield: 88.0%

: 56061-88-2
Triphenyl<(2-tetrahydropyranyloxy)methyl>phosphonium chloride

: 173483-59-5
2-[N-(tert-Butyloxycarbonyl)-N-(formylmethyl)]amino-4-benzyloxy-1-bromo-7-methoxynaphthalene

: (4-Benzyloxy-1-bromo-7-methoxy-naphthalen-2-yl)-[(E)-3-(tetrahydro-pyran-2-yloxy)-allyl]-carbamic acid tert-butyl ester

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 5 min, 2.) -78 deg C, 20 min; 24 deg C, 5 h;
DOI:10.1021/jo952033g

Reference yield:

: 56061-88-2
Triphenyl<(2-tetrahydropyranyloxy)methyl>phosphonium chloride

: 129918-06-5
2--4-(benzyloxy)-1-bromonaphthalene

: 139975-99-8,139976-00-4
2-amino>-4-(benzyloxy)-1-bromonaphthalene

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; Yield given. Multistep reaction; 1.a) THF, Pentane, -78 deg C, 5 min, b) up to 24 deg C, 30 min, 2.a) THF, -78 deg C, 1.5 h, b) 24 deg C, 24 h;
DOI:10.1021/jo00036a023