(S)-(-)-1-butoxymethyl-4-acetyl-1-cyclohexene

Base Information

Chemical Name:(S)-(-)-1-butoxymethyl-4-acetyl-1-cyclohexene
CAS No.:146659-09-8
Molecular Formula:C₁₃H₂₂O₂
Molecular Weight:210.316
Hs Code.:

Synonyms:(S)-(-)-1-butoxymethyl-4-acetyl-1-cyclohexene

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Chemical Property of (S)-(-)-1-butoxymethyl-4-acetyl-1-cyclohexene

Chemical Property:

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Technology Process of (S)-(-)-1-butoxymethyl-4-acetyl-1-cyclohexene

There total 8 articles about (S)-(-)-1-butoxymethyl-4-acetyl-1-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7785-70-8,25766-18-1
(+)-α-pinene

: 146659-09-8
(S)-(-)-1-butoxymethyl-4-acetyl-1-cyclohexene

Guidance literature:: Multi-step reaction with 6 steps

2: 35 percent / potassium bicarbonate, benzonitrile, 30percent hydrogen peroxide / methanol / 24 h / Ambient temperature

3: ammonium nitrate / nitromethane / 4 h / 80 °C

4: 90 percent / sodium hydride / tetrahydrofuran / 10 h / Heating

5: 55 percent / methyltrioctylammonium chloride, magnesium monoperoxyphthalic acid / H₂O; CHCl₃ / 5 h / 50 °C

6: 1) ozone, 2) zinc dust, sodium acetate, sodium iodide / 1) CH₂Cl₂, -78 deg C, 2) glacial acetic acid, 0 deg C up to r.t., overnight

With ammonium nitrate; dihydrogen peroxide; sodium acetate; Aliquat 336; sodium hydride; potassium hydrogencarbonate; magnesium monoperoxyphthalate hexahydrate; ozone; benzonitrile; sodium iodide; zinc; In tetrahydrofuran; methanol; nitromethane; chloroform; water;
DOI:10.1016/S0040-4020(01)86265-7

Reference yield:

: 18172-67-3,19902-08-0,25719-60-2
beta-pinene

: 146659-09-8
(S)-(-)-1-butoxymethyl-4-acetyl-1-cyclohexene

Guidance literature:: Multi-step reaction with 5 steps

1: 35 percent / potassium bicarbonate, benzonitrile, 30percent hydrogen peroxide / methanol / 24 h / Ambient temperature

2: ammonium nitrate / nitromethane / 4 h / 80 °C

3: 90 percent / sodium hydride / tetrahydrofuran / 10 h / Heating

4: 55 percent / methyltrioctylammonium chloride, magnesium monoperoxyphthalic acid / H₂O; CHCl₃ / 5 h / 50 °C

5: 1) ozone, 2) zinc dust, sodium acetate, sodium iodide / 1) CH₂Cl₂, -78 deg C, 2) glacial acetic acid, 0 deg C up to r.t., overnight

With ammonium nitrate; dihydrogen peroxide; sodium acetate; Aliquat 336; sodium hydride; potassium hydrogencarbonate; magnesium monoperoxyphthalate hexahydrate; ozone; benzonitrile; sodium iodide; zinc; In tetrahydrofuran; methanol; nitromethane; chloroform; water;
DOI:10.1016/S0040-4020(01)86265-7

Reference yield:

: 127-91-3,25719-60-2
(1R,5R)-(+)-β-pinene

: 146659-09-8
(S)-(-)-1-butoxymethyl-4-acetyl-1-cyclohexene

Guidance literature:: Multi-step reaction with 5 steps

1: 35 percent / potassium bicarbonate, benzonitrile, 30percent hydrogen peroxide / methanol / 24 h / Ambient temperature

2: ammonium nitrate / nitromethane / 4 h / 80 °C

3: 90 percent / sodium hydride / tetrahydrofuran / 10 h / Heating

4: 55 percent / methyltrioctylammonium chloride, magnesium monoperoxyphthalic acid / H₂O; CHCl₃ / 5 h / 50 °C

5: 1) ozone, 2) zinc dust, sodium acetate, sodium iodide / 1) CH₂Cl₂, -78 deg C, 2) glacial acetic acid, 0 deg C up to r.t., overnight

With ammonium nitrate; dihydrogen peroxide; sodium acetate; Aliquat 336; sodium hydride; potassium hydrogencarbonate; magnesium monoperoxyphthalate hexahydrate; ozone; benzonitrile; sodium iodide; zinc; In tetrahydrofuran; methanol; nitromethane; chloroform; water;
DOI:10.1016/S0040-4020(01)86265-7