(R)-2-[(S)-(tert-Butyl-dimethyl-silanyloxy)-((4S,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)-methyl]-N-((S)-2-oxo-azepan-3-yl)-butyramide

Base Information

• Chemical Name: (R)-2-[(S)-(tert-Butyl-dimethyl-silanyloxy)-((4S,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)-methyl]-N-((S)-2-oxo-azepan-3-yl)-butyramide
• CAS No.: 870093-62-2
• Molecular Formula: C₂₄H₄₄N₂O₅Si
• Molecular Weight: 468.709

Synonyms:(R)-2-[(S)-(tert-Butyl-dimethyl-silanyloxy)-((4S,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)-methyl]-N-((S)-2-oxo-azepan-3-yl)-butyramide

Chemical Property of (R)-2-[(S)-(tert-Butyl-dimethyl-silanyloxy)-((4S,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)-methyl]-N-((S)-2-oxo-azepan-3-yl)-butyramide

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Technology Process of (R)-2-[(S)-(tert-Butyl-dimethyl-silanyloxy)-((4S,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)-methyl]-N-((S)-2-oxo-azepan-3-yl)-butyramide

There total 1 articles about (R)-2-[(S)-(tert-Butyl-dimethyl-silanyloxy)-((4S,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)-methyl]-N-((S)-2-oxo-azepan-3-yl)-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-2-[(S)-(tert-Butyl-dimethyl-silanyloxy)-((4S,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)-methyl]-butyric acid + 2-aminocaprolactam (21568-87-6) → (R)-2-[(S)-(tert-Butyl-dimethyl-silanyloxy)-((4S,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolan-4-yl)-methyl]-N-((S)-2-oxo-azepan-3-yl)-butyramide (870093-62-2)

Guidance literature:

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 25 ℃; for 3h;

DOI:10.1021/jo0516032

upstream raw materials:

2-aminocaprolactam

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