C₄₁H₄₆INO₇

Base Information

Chemical Name:C₄₁H₄₆INO₇
CAS No.:1379450-06-2
Molecular Formula:C₄₁H₄₆INO₇
Molecular Weight:791.723
Hs Code.:

C<sub>41</sub>H<sub>46</sub>INO<sub>7</sub>

Synonyms:C₄₁H₄₆INO₇

Suppliers and Price of C₄₁H₄₆INO₇

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₁H₄₆INO₇

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₁H₄₆INO₇

There total 12 articles about C₄₁H₄₆INO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1379450-05-1
C₄₂H₄₉NO₁₀S

: 1379450-06-2
C₄₁H₄₆INO₇

Guidance literature:: With sodium iodide; In acetone; at 25 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ja301326k

Reference yield:

: 1379449-94-1
C₂₁H₃₂N₂O₆

: 1379450-06-2
C₄₁H₄₆INO₇

Guidance literature:: Multi-step reaction with 9 steps

1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C

3: tetrahydrofuran / 0 - 25 °C / Inert atmosphere; Molecular sieve

4: pyridinium chlorochromate / dichloromethane / 4 h / 25 °C / Inert atmosphere; Molecular sieve

5: 2,6-di-tert-butyl-pyridine / nitromethane / 2 h / -20 °C / Inert atmosphere; Molecular sieve

6: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 16 h / 45 °C / Inert atmosphere

7: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

8: dmap; triethylamine / dichloromethane / 0 - 18 °C / Inert atmosphere

9: sodium iodide / acetone / 24 h / 25 °C / Inert atmosphere

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-pyridine; pyridine hydrogenfluoride; triethylamine; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; pyridinium chlorochromate; sodium iodide; In tetrahydrofuran; nitromethane; dichloromethane; N,N-dimethyl-formamide; acetone; 5: Friedel Crafts acylation / 6: Stille coupling;
DOI:10.1021/ja301326k

Reference yield:

: 1379449-81-6
C₁₈H₂₈N₂O₆

: 1379450-06-2
C₄₁H₄₆INO₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 6 h / 0 °C

2.1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C

4.1: tetrahydrofuran / 0 - 25 °C / Inert atmosphere; Molecular sieve

5.1: pyridinium chlorochromate / dichloromethane / 4 h / 25 °C / Inert atmosphere; Molecular sieve

6.1: 2,6-di-tert-butyl-pyridine / nitromethane / 2 h / -20 °C / Inert atmosphere; Molecular sieve

7.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 16 h / 45 °C / Inert atmosphere

8.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

9.1: dmap; triethylamine / dichloromethane / 0 - 18 °C / Inert atmosphere

10.1: sodium iodide / acetone / 24 h / 25 °C / Inert atmosphere

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-pyridine; sodium hydride; pyridine hydrogenfluoride; triethylamine; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; pyridinium chlorochromate; sodium iodide; In tetrahydrofuran; nitromethane; dichloromethane; N,N-dimethyl-formamide; acetone; 6.1: Friedel Crafts acylation / 7.1: Stille coupling;
DOI:10.1021/ja301326k