1,1,3,3-tetrakis(salicylidene-3-iminopropyl)butylenediamine

Base Information

• Chemical Name: 1,1,3,3-tetrakis(salicylidene-3-iminopropyl)butylenediamine
• CAS No.: 1028904-08-6
• Molecular Formula: C₄₄H₅₆N₆O₄
• Molecular Weight: 732.966
• Mol file: 1028904-08-6.mol

Synonyms:1,1,3,3-tetrakis(salicylidene-3-iminopropyl)butylenediamine

Chemical Property of 1,1,3,3-tetrakis(salicylidene-3-iminopropyl)butylenediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1,3,3-tetrakis(salicylidene-3-iminopropyl)butylenediamine

There total 2 articles about 1,1,3,3-tetrakis(salicylidene-3-iminopropyl)butylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

salicylaldehyde (90-02-8) + N,N,N',N'-tetra(3-aminopropyl)-1,4-butanediamine (120239-63-6) → 1,1,3,3-tetrakis(salicylidene-3-iminopropyl)butylenediamine (1028904-08-6)

Guidance literature:

In ethanol; at 50 ℃; for 2h;

DOI:10.1016/j.ica.2012.08.007

Reference yield:

3,3′,3″,3′″-(butane-1,4-diylbis(azanetriyl))tetrapropanenitrile → 1,1,3,3-tetrakis(salicylidene-3-iminopropyl)butylenediamine (1028904-08-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide; hydrogen / methanol / 8 h / 20 °C / 5171.62 Torr

2: toluene / Inert atmosphere

With hydrogen; sodium hydroxide; In methanol; toluene;

DOI:10.1080/00397911.2014.941501

upstream raw materials:

salicylaldehyde

N,N,N',N'-tetra(3-aminopropyl)-1,4-butanediamine