C₂B₁₀H₁₁C₆H₄CH₂CH(CN)NC(C₆H₅)2

Base Information

Chemical Name:C₂B₁₀H₁₁C₆H₄CH₂CH(CN)NC(C₆H₅)2
CAS No.:180193-11-7
Molecular Formula:C₂₄H₂₈B₁₀N₂
Molecular Weight:452.61
Hs Code.:

C<sub>2</sub>B<sub>10</sub>H<sub>11</sub>C<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>CH(CN)NC(C<sub>6</sub>H<sub>5</sub>)2

Synonyms:C₂B₁₀H₁₁C₆H₄CH₂CH(CN)NC(C₆H₅)2

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Chemical Property of C₂B₁₀H₁₁C₆H₄CH₂CH(CN)NC(C₆H₅)2

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Technology Process of C₂B₁₀H₁₁C₆H₄CH₂CH(CN)NC(C₆H₅)2

There total 1 articles about C₂B₁₀H₁₁C₆H₄CH₂CH(CN)NC(C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 150174-85-9
1-{p-(alpha-bromo)tolyl}-1,2-dicarba-closo-dodecaborane

: 70591-20-7
N-(diphenylmethylene)aminoacetonitrile

: 180193-11-7
C₂B₁₀H₁₁C₆H₄CH₂CH(CN)NC(C₆H₅)2

Guidance literature:: With tetrabutylammomium bromide; potassium carbonate; In acetonitrile; Ar-atmosphere; addn. of excess K2CO3 and 0.3 equiv. Bu4NBr to equimolar amts. of borane and nitrile, refluxing for 4 h; filtration, washing (CH2Cl2), chromy. (SiO2, hexanes/EtOAc=10:1), recrystn. (hexanes/EtOAc=5:1); elem. anal.;
DOI:10.1021/ic9511229

Reference yield: 79.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 180193-11-7
C₂B₁₀H₁₁C₆H₄CH₂CH(CN)NC(C₆H₅)2

: 7664-93-9
sulfuric acid

: 146490-19-9
4-{1,2-dicarba-closo-dodecaboran⁽¹²⁾-1-yl}phenylalanine

Guidance literature:: In benzene; stirring borane with excess 6 N HCl (room temp., 17 h), extn. of org. layer into ether, drying of combined org. layers, evapn., chromy. (SiO2, CHCl3/MeOH=10:1), stirring with 75% H2SO4 (95°C, 24 h); cooling in ice-water bath, washing (H2O), drying (vac.), HPLC (reversed C8-phase, MeOH/H2O=8.5:1.5); elem. anal.;
DOI:10.1021/ic9511229