1-allyl-5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)pyridinium-3-olate

Base Information

Chemical Name:1-allyl-5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)pyridinium-3-olate
CAS No.:937183-45-4
Molecular Formula:C₅₃H₅₇N₃O₉
Molecular Weight:880.05
Hs Code.:

1-allyl-5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)pyridinium-3-olate

Synonyms:1-allyl-5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)pyridinium-3-olate

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Chemical Property of 1-allyl-5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)pyridinium-3-olate

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Technology Process of 1-allyl-5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)pyridinium-3-olate

There total 1 articles about 1-allyl-5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)pyridinium-3-olate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 937183-39-6
tert-butyl (3S,5S,6R)-3-(4-iodo-3-oxobutyl)-2-oxo-5,6-diphenylmorpholine-4-carboxylate

: 107-11-9,30551-89-4
1-amino-2-propene

: 937183-45-4
1-allyl-5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)pyridinium-3-olate

Guidance literature:: tert-butyl (3S,5S,6R)-3-(4-iodo-3-oxobutyl)-2-oxo-5,6-diphenylmorpholine-4-carboxylate; 1-amino-2-propene; With sodium carbonate; In acetonitrile; at 20 ℃; for 2h;

With oxygen; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 96h; Further stages.;
DOI:10.1021/jo070136g

Reference yield: 87.0%

: 937183-45-4
1-allyl-5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)pyridinium-3-olate

: 937183-46-5
5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)-3-hydroxypyridine

Guidance literature:: With Thiosalicylic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; at 20 ℃; for 1.3h;
DOI:10.1021/jo070136g

Reference yield:

: 937183-45-4
1-allyl-5-{2-[(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]ethyl}-4-([(3S,5S,6R)-4-(tert-butoxycarbonyl)-2-oxo-5,6-diphenylmorpholin-3-yl]methyl)pyridinium-3-olate

: 937183-43-2
C₇₅H₈₂N₄O₁₄

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 2-mercaptobenzoic acid / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / CH₂Cl₂ / 1.3 h / 20 °C

2: 58 percent / acetonitrile / 20 h / Heating

With Thiosalicylic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; acetonitrile;
DOI:10.1021/jo070136g