C₃₅H₄₈ClN₉O₇S

Base Information

Chemical Name:C₃₅H₄₈ClN₉O₇S
CAS No.:1353629-11-4
Molecular Formula:C₃₅H₄₈ClN₉O₇S
Molecular Weight:774.341
Hs Code.:

C<sub>35</sub>H<sub>48</sub>ClN<sub>9</sub>O<sub>7</sub>S

Synonyms:C₃₅H₄₈ClN₉O₇S

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Chemical Property of C₃₅H₄₈ClN₉O₇S

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Technology Process of C₃₅H₄₈ClN₉O₇S

There total 9 articles about C₃₅H₄₈ClN₉O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 217806-26-3
tert-butyl N-(azetidin-3-yl)carbamate hydrochloride

: 1353629-09-0
C₂₇H₃₃Cl₂N₇O₅S

: 1353629-11-4
C₃₅H₄₈ClN₉O₇S

Guidance literature:: With triethylamine; In methanol; at 70 ℃; for 18h;

Reference yield:

: 26250-84-0
(S)-(-)-1-(tert-butoxycarbonyl)-2-piperidinecarboxylic acid

: 1353629-11-4
C₃₅H₄₈ClN₉O₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 4 h

2.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran; hexanes / -78 - -40 °C

2.2: -78 - -40 °C

2.3: -78 - 20 °C

3.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

4.1: sodium methylate / methanol / 5 h / 78 °C

5.1: trichlorophosphate / 3 h / 100 °C

6.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 °C

6.2: 0.67 h / 20 °C / Cooling with ice

7.1: sodium hydrogencarbonate / acetonitrile; water / 18 h / 20 °C

8.1: triethylamine / methanol / 18 h / 70 °C

With oxalyl dichloride; sodium bis(trimethylsilyl)amide; sodium methylate; hydrazinium monoacetate; sodium hydrogencarbonate; caesium carbonate; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; hexanes; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 203056-27-3
tert-butyl (2S)-2-{[methoxy(methyl)amino]-carbonyl}piperidine-1-carboxylate

: 1353629-11-4
C₃₅H₄₈ClN₉O₇S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 0.42 h / -78 - -20 °C / Inert atmosphere

1.2: 3.08 h / -78 - -45 °C

1.3: -78 - 20 °C

2.1: hydrazinium monoacetate / ethanol / 16 h / 20 °C

3.1: sodium methylate / methanol / 5 h / 78 °C

4.1: trichlorophosphate / 3 h / 100 °C

5.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 °C

5.2: 0.67 h / 20 °C / Cooling with ice

6.1: sodium hydrogencarbonate / acetonitrile; water / 18 h / 20 °C

7.1: triethylamine / methanol / 18 h / 70 °C

With oxalyl dichloride; sodium bis(trimethylsilyl)amide; sodium methylate; hydrazinium monoacetate; sodium hydrogencarbonate; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;