diosgenyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3,5-dinitrobenzamido)-β-D-glucopyranoside

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Chemical Name:diosgenyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3,5-dinitrobenzamido)-β-D-glucopyranoside
CAS No.:1202534-47-1
Molecular Formula:C₄₆H₆₁N₃O₁₅
Molecular Weight:896.001
Hs Code.:

Synonyms:diosgenyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3,5-dinitrobenzamido)-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diosgenyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3,5-dinitrobenzamido)-β-D-glucopyranoside

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Technology Process of diosgenyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3,5-dinitrobenzamido)-β-D-glucopyranoside

There total 1 articles about diosgenyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3,5-dinitrobenzamido)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1028758-85-1
diosgenyl 3,4,6-tri-O-acetyl-2-amino-2-deoxy-D-glucopyranoside

: 99-34-3
3,5-dinitrobenzoic acid

: 1202534-47-1
diosgenyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3,5-dinitrobenzamido)-β-D-glucopyranoside

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2009.09.046

Reference yield: 78.0%

: 1202534-47-1
diosgenyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3,5-dinitrobenzamido)-β-D-glucopyranoside

: 1202534-51-7
diosgenyl 2-deoxy-2-(3,5-dinitrobenzamido)-β-D-glucopyranoside

Guidance literature:: diosgenyl 3,4,6-tri-O-acetyl-2-deoxy-2-(3,5-dinitrobenzamido)-β-D-glucopyranoside; With sodium methylate; In methanol; dichloromethane; at 20 ℃; Inert atmosphere;

In methanol; dichloromethane;
DOI:10.1016/j.bmc.2009.09.046