Technology Process of C11H14FN3S
There total 5 articles about C11H14FN3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C36H40FN3O4S;
With
trifluoroacetic acid;
for 22h;
Reflux;
With
potassium carbonate;
In
water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogen / palladium 10% on activated carbon / ethanol / 8 h / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 7.5 h / 50 °C
3: toluene-4-sulfonic acid / toluene / 14 h / Reflux
4: trichlorophosphate / 23 h / 20 °C
5: toluene / 5.5 h / 20 - 100 °C
6: trifluoroacetic acid / 22 h / Reflux
With
hydrogen; potassium carbonate; toluene-4-sulfonic acid; trifluoroacetic acid; trichlorophosphate;
palladium 10% on activated carbon;
In
ethanol; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / toluene / 14 h / Reflux
2: trichlorophosphate / 23 h / 20 °C
3: toluene / 5.5 h / 20 - 100 °C
4: trifluoroacetic acid / 22 h / Reflux
With
toluene-4-sulfonic acid; trifluoroacetic acid; trichlorophosphate;
In
toluene;