tert-Butyl (4S,2Z)-4,5-[N-(2,4,6-trimethylphenylsulfonyl)epimino]pent-2-enoate

Base Information

Chemical Name:tert-Butyl (4S,2Z)-4,5-[N-(2,4,6-trimethylphenylsulfonyl)epimino]pent-2-enoate
CAS No.:1085965-64-5
Molecular Formula:C₁₈H₂₅NO₄S
Molecular Weight:351.467
Hs Code.:

Synonyms:tert-Butyl (4S,2Z)-4,5-[N-(2,4,6-trimethylphenylsulfonyl)epimino]pent-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-Butyl (4S,2Z)-4,5-[N-(2,4,6-trimethylphenylsulfonyl)epimino]pent-2-enoate

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Technology Process of tert-Butyl (4S,2Z)-4,5-[N-(2,4,6-trimethylphenylsulfonyl)epimino]pent-2-enoate

There total 1 articles about tert-Butyl (4S,2Z)-4,5-[N-(2,4,6-trimethylphenylsulfonyl)epimino]pent-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (o-MePhO₂)2P(O)CH₂CO₂t-Bu

: C₁₂H₁₅NSO₃

: 1085965-64-5
tert-Butyl (4S,2Z)-4,5-[N-(2,4,6-trimethylphenylsulfonyl)epimino]pent-2-enoate

: 1085965-87-2
tert-Butyl (4S,2E)-4,5-[N-(2,4,6-trimethylphenylsulfonyl)epimino]pent-2-enoate

Guidance literature:: (o-MePhO₂)2P(O)CH₂CO₂t-Bu; With 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In tetrahydrofuran; at 4 ℃; for 0.166667h; Inert atmosphere;

C₁₂H₁₅NSO₃; In tetrahydrofuran; at -78 - -40 ℃;
DOI:10.1021/jm800930w

Reference yield: 90.0%

: 1085965-64-5
tert-Butyl (4S,2Z)-4,5-[N-(2,4,6-trimethylphenylsulfonyl)epimino]pent-2-enoate

: 5674-02-2
2-methylpropylmagnesium chloride

: 1085965-65-6
tert-butyl (2R,3E)-2-isobutyl-5-[N-(2,4,6-trimethylphenylsulfonyl)amino]pent-3-enoate

Guidance literature:: 2-methylpropylmagnesium chloride; With copper(l) cyanide; lithium chloride; In tetrahydrofuran; at -78 - 4 ℃;

tert-Butyl (4S,2Z)-4,5-[N-(2,4,6-trimethylphenylsulfonyl)epimino]pent-2-enoate; In tetrahydrofuran; at -78 ℃; for 0.5h;
DOI:10.1021/jm800930w